1-Methyl-3-[2-(phenylselanyl)prop-2-en-1-yl]-1H-pyrrole

Base Information

Chemical Name:1-Methyl-3-[2-(phenylselanyl)prop-2-en-1-yl]-1H-pyrrole
CAS No.:87728-79-8
Molecular Formula:C₁₄H₁₅NSe
Molecular Weight:276.24
Hs Code.:
DSSTox Substance ID:DTXSID20527229
Wikidata:Q82396362

Synonyms:87728-79-8;DTXSID20527229;1-Methyl-3-[2-(phenylselanyl)prop-2-en-1-yl]-1H-pyrrole

Suppliers and Price of 1-Methyl-3-[2-(phenylselanyl)prop-2-en-1-yl]-1H-pyrrole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 1-Methyl-3-[2-(phenylselanyl)prop-2-en-1-yl]-1H-pyrrole

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:4
Exact Mass:277.03697
Heavy Atom Count:16
Complexity:233

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1C=CC(=C1)CC(=C)[Se]C2=CC=CC=C2

Technology Process of 1-Methyl-3-[2-(phenylselanyl)prop-2-en-1-yl]-1H-pyrrole

There total 2 articles about 1-Methyl-3-[2-(phenylselanyl)prop-2-en-1-yl]-1H-pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 96-54-8
N-Methylpyrrole

: 87728-67-4
2-(phenylseleno)-3-bromo-1-propene

: 87728-78-7
1-Methyl-2-(2-phenylselanyl-allyl)-1H-pyrrole

: 87728-79-8
1-Methyl-3-(2-phenylselanyl-allyl)-1H-pyrrole

Guidance literature:: With silver perchlorate; sodium carbonate; In nitromethane; at -15 ℃; for 6h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/jo00174a017

Reference yield:

: 34837-55-3
Phenylselenyl bromide

: 87728-79-8
1-Methyl-3-(2-phenylselanyl-allyl)-1H-pyrrole

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / CH₂Cl₂ / 1.) -78 deg C, 2.) room temp., 0.5 h

2: silver perchlorate, Na₂CO₃ / nitromethane / 6 h / -15 °C

With silver perchlorate; sodium carbonate; In nitromethane; dichloromethane;
DOI:10.1021/jo00174a017