2-(2,3-Dichloroanilino)ethan-1-ol

Base Information

Chemical Name:2-(2,3-Dichloroanilino)ethan-1-ol
CAS No.:87762-19-4
Molecular Formula:C8H9Cl2NO
Molecular Weight:206.072
Hs Code.:
DSSTox Substance ID:DTXSID70528125
Wikidata:Q82397508

Synonyms:2-(2,3-Dichloroanilino)ethan-1-ol;87762-19-4;SCHEMBL6414632;DTXSID70528125;RSGHDONOLAYJET-UHFFFAOYSA-N;AKOS009216031;2-(2,3-Dichloro-phenylamino)-ethanol

Suppliers and Price of 2-(2,3-Dichloroanilino)ethan-1-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(2,3-Dichloroanilino)ethan-1-ol

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:205.0061193
Heavy Atom Count:12
Complexity:134

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(C(=C1)Cl)Cl)NCCO

Technology Process of 2-(2,3-Dichloroanilino)ethan-1-ol

There total 4 articles about 2-(2,3-Dichloroanilino)ethan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₉H₈Cl₃NO₂

: 87762-19-4
2-<(2,3-dichlorophenyl)amino>ethanol

Guidance literature:: With potassium hydroxide; In ethanol; at 90 ℃; for 4h;
DOI:10.1016/j.bmcl.2005.08.004

Reference yield:

: 608-27-5
2,3-dichloroaniline

: 87762-19-4
2-<(2,3-dichlorophenyl)amino>ethanol

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / CH₂Cl₂ / 16 h / 20 °C

2: KOH / ethanol / 4 h / 90 °C

With pyridine; potassium hydroxide; In ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2005.08.004

Reference yield:

: 87762-15-0
2-(2,3-dichlorophenoxy)-N-(2-hydroxyethyl)acetamide

: 87762-19-4
2-<(2,3-dichlorophenyl)amino>ethanol

Guidance literature:: With 18-crown-6 ether; water; potassium hydride; Yield given. Multistep reaction; 1) THF, -20 to 0 deg C, 1 h, 2) THF;
DOI:10.1021/jo00173a076