Tricyclo(6.2.0.0(3,6))deca-1(8),3(6)-diene-2,7-dione

Base Information

Chemical Name:Tricyclo(6.2.0.0(3,6))deca-1(8),3(6)-diene-2,7-dione
CAS No.:87258-06-8
Molecular Formula:C₁₀H₈O₂
Molecular Weight:160.172
Hs Code.:
DSSTox Substance ID:DTXSID00236241
Nikkaji Number:J600.087H
Wikidata:Q83118179

Synonyms:87258-06-8;Tricyclo(6.2.0.0(3,6))deca-1(8),3(6)-diene-2,7-dione;Tricyclo[6.2.0.0(3,6)]deca-1(8),3(6)-diene-2,7-dione;Tricyclo[6.2.0.03,6]deca-1,4-diene-2,7-dione;DTXSID00236241

Suppliers and Price of Tricyclo(6.2.0.0(3,6))deca-1(8),3(6)-diene-2,7-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of Tricyclo(6.2.0.0(3,6))deca-1(8),3(6)-diene-2,7-dione

Chemical Property:

Vapor Pressure:0.000675mmHg at 25°C
Boiling Point:308.6°Cat760mmHg
Flash Point:115.4°C
Density:1.35g/cm³
XLogP3:0.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:160.052429494
Heavy Atom Count:12
Complexity:313

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC2=C1C(=O)C3=C(C2=O)CC3

Technology Process of Tricyclo(6.2.0.0(3,6))deca-1(8),3(6)-diene-2,7-dione

There total 5 articles about Tricyclo(6.2.0.0(3,6))deca-1(8),3(6)-diene-2,7-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 87258-05-7
Tricyclo[6.2.0.0^3,6]deca-1⁽⁸⁾,2,6-triene-2,7-diol

: 87258-06-8
<2,3:5,6>dicyclobuta-p-benzoquinone

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In acetonitrile; Ambient temperature;
DOI:10.1016/S0040-4039(00)81755-4

Reference yield:

: 94499-49-7
(3S,6R)-Tricyclo[6.2.0.0^3,6]dec-1⁽⁸⁾-ene-2,7-dione

: 87258-06-8
<2,3:5,6>dicyclobuta-p-benzoquinone

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / 1,8-diazabicyclo<5.4.0>undec-7-ene / tetrahydrofuran / Ambient temperature

2: 74 percent / 2,3-dichloro-5,6-dicyano-p-benzoquinone / acetonitrile / Ambient temperature

With 1,8-diazabicyclo[5.4.0]undec-7-ene; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; acetonitrile;
DOI:10.1016/S0040-4039(00)81755-4

Reference yield:

: 77627-56-6
bicyclo<4.2.0>oct-3-ene-2,5-dione

: 87258-06-8
<2,3:5,6>dicyclobuta-p-benzoquinone

Guidance literature:: Multi-step reaction with 3 steps

1: 2) SeO₂ / 1.) CH₂Cl₂, 0 degC, irradiation; 2.) ethyl acetate, reflux, 3 h.

2: 83 percent / 1,8-diazabicyclo<5.4.0>undec-7-ene / tetrahydrofuran / Ambient temperature

3: 74 percent / 2,3-dichloro-5,6-dicyano-p-benzoquinone / acetonitrile / Ambient temperature

With selenium(IV) oxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; acetonitrile;
DOI:10.1016/S0040-4039(00)81755-4