Benzene, [[(1,3-dimethyl-4-phenyl-3-butenyl)oxy]methyl]-, (R)-

Base Information

Chemical Name:Benzene, [[(1,3-dimethyl-4-phenyl-3-butenyl)oxy]methyl]-, (R)-
CAS No.:87841-62-1
Molecular Formula:C₁₉H₂₂O
Molecular Weight:266.383
Hs Code.:

Synonyms:

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Chemical Property of Benzene, [[(1,3-dimethyl-4-phenyl-3-butenyl)oxy]methyl]-, (R)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of Benzene, [[(1,3-dimethyl-4-phenyl-3-butenyl)oxy]methyl]-, (R)-

There total 9 articles about Benzene, [[(1,3-dimethyl-4-phenyl-3-butenyl)oxy]methyl]-, (R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 87841-58-5
(2S,3R)-2-(Benzoyloxy)-3-hydroxy-4-methyl-5-phenylpent-4-ene

: 87841-62-1
C₁₉H₂₂O

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / pyridine / 120 h / Ambient temperature

2: 55 percent / NaOH / ethane-1,2-diol; H₂O / 3 h / 40 °C

3: LiAlH₄

With pyridine; sodium hydroxide; lithium aluminium tetrahydride; In water; ethylene glycol;
DOI:10.1021/jo00177a031

Reference yield:

: 87841-57-4
Toluene-4-sulfonic acid (E)-(1S,2R)-2-hydroxy-1,3-dimethyl-4-phenyl-but-3-enyl ester

: 87841-62-1
(2R)-2-(Benzyloxy)-4-methyl-5-phenylpent-4-ene

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / NaOH / ethane-1,2-diol; H₂O / 3 h / Ambient temperature

2: 80 percent / diisobutylaluminum hydride / tetrahydrofuran; hexane / 3 h / -50 °C

3: 1.) NaH / 1.) DMF, 40 deg C, 3 h, 2.) 2 h

With sodium hydroxide; sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; hexane; water; ethylene glycol;
DOI:10.1021/jo00177a031

Reference yield:

: 87841-59-6
Benzoic acid (E)-(1S,2R)-1,3-dimethyl-4-phenyl-2-(toluene-4-sulfonyloxy)-but-3-enyl ester

: 87841-62-1
C₁₉H₂₂O

Guidance literature:: Multi-step reaction with 3 steps

1: 55 percent / NaOH / ethane-1,2-diol; H₂O / 3 h / 40 °C

2: LiAlH₄

With sodium hydroxide; lithium aluminium tetrahydride; In water; ethylene glycol;
DOI:10.1021/jo00177a031