3-Thiomorpholinecarboxylic acid, 2,2-dimethyl-4-[[4-[[6-[(tetrahydro-2H-pyran-2-yl)oxy]-2-hexynyl]oxy]phen yl]sulfonyl]-, methyl ester, (3S)-

Base Information

Chemical Name:3-Thiomorpholinecarboxylic acid, 2,2-dimethyl-4-[[4-[[6-[(tetrahydro-2H-pyran-2-yl)oxy]-2-hexynyl]oxy]phen yl]sulfonyl]-, methyl ester, (3S)-
CAS No.:878807-82-0
Molecular Formula:C₂₅H₃₅NO₇S₂
Molecular Weight:525.687
Hs Code.:

3-Thiomorpholinecarboxylic acid,
2,2-dimethyl-4-[[4-[[6-[(tetrahydro-2H-pyran-2-yl)oxy]-2-hexynyl]oxy]phen
yl]sulfonyl]-, methyl ester, (3S)-

Synonyms:

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Chemical Property of 3-Thiomorpholinecarboxylic acid, 2,2-dimethyl-4-[[4-[[6-[(tetrahydro-2H-pyran-2-yl)oxy]-2-hexynyl]oxy]phen yl]sulfonyl]-, methyl ester, (3S)-

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Technology Process of 3-Thiomorpholinecarboxylic acid, 2,2-dimethyl-4-[[4-[[6-[(tetrahydro-2H-pyran-2-yl)oxy]-2-hexynyl]oxy]phen yl]sulfonyl]-, methyl ester, (3S)-

There total 4 articles about 3-Thiomorpholinecarboxylic acid, 2,2-dimethyl-4-[[4-[[6-[(tetrahydro-2H-pyran-2-yl)oxy]-2-hexynyl]oxy]phen yl]sulfonyl]-, methyl ester, (3S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 192329-86-5
methyl (3S)-2,2-dimethylthiomorpholine-3-carboxylate

: 878807-82-0
(S)-2,2-Dimethyl-4-{4-[6-(tetrahydro-pyran-2-yloxy)-hex-2-ynyloxy]-benzenesulfonyl}-thiomorpholine-3-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: BTSA

2: PPh₃; DEAD

With benzothiazole-2-sulphonic acid; triphenylphosphine; diethylazodicarboxylate; 2: Mitsunobu alkylation;
DOI:10.1016/j.bmcl.2005.12.020

Reference yield:

: 62992-46-5
1-(tetrahydropyranyloxy)-4-pentyn

: 878807-82-0
(S)-2,2-Dimethyl-4-{4-[6-(tetrahydro-pyran-2-yloxy)-hex-2-ynyloxy]-benzenesulfonyl}-thiomorpholine-3-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: n-BuLi

2: PPh₃; DEAD

With n-butyllithium; triphenylphosphine; diethylazodicarboxylate; 2: Mitsunobu alkylation;
DOI:10.1016/j.bmcl.2005.12.020

Reference yield:

: 4025-67-6
4-hydroxybenzene-1-sulfonyl chloride

: 878807-82-0
(S)-2,2-Dimethyl-4-{4-[6-(tetrahydro-pyran-2-yloxy)-hex-2-ynyloxy]-benzenesulfonyl}-thiomorpholine-3-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: BTSA

2: PPh₃; DEAD

With benzothiazole-2-sulphonic acid; triphenylphosphine; diethylazodicarboxylate; 2: Mitsunobu alkylation;
DOI:10.1016/j.bmcl.2005.12.020