3-[Methyl(2-methylprop-1-en-1-yl)amino]cyclohex-2-en-1-one

Base Information

Chemical Name:3-[Methyl(2-methylprop-1-en-1-yl)amino]cyclohex-2-en-1-one
CAS No.:87883-84-9
Molecular Formula:C₁₁H₁₇NO
Molecular Weight:179.262
Hs Code.:
DSSTox Substance ID:DTXSID80529123

Synonyms:87883-84-9;DTXSID80529123;3-[Methyl(2-methylprop-1-en-1-yl)amino]cyclohex-2-en-1-one

Suppliers and Price of 3-[Methyl(2-methylprop-1-en-1-yl)amino]cyclohex-2-en-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of 3-[Methyl(2-methylprop-1-en-1-yl)amino]cyclohex-2-en-1-one

Chemical Property:

XLogP3:2.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:179.131014166
Heavy Atom Count:13
Complexity:259

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=CN(C)C1=CC(=O)CCC1)C

Technology Process of 3-[Methyl(2-methylprop-1-en-1-yl)amino]cyclohex-2-en-1-one

There total 3 articles about 3-[Methyl(2-methylprop-1-en-1-yl)amino]cyclohex-2-en-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 87883-67-8
3--2-propenyl>-amino>cyclohex-2-enone

: 87883-83-8
3-cyclohex-2-enone

: 87883-84-9
3-cyclohex-2-enone

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; 1.) 14h, 25 deg C 2.) 12h, reflux;
DOI:10.1021/jo00176a002

Reference yield:

: 55998-74-8
3-(methylamino)-2-cyclohexen-1-one

: 87883-84-9
3-cyclohex-2-enone

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / NaH / tetrahydrofuran / 1h, reflux -> 25 deg C, 24h

2: 31 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 1.) 14h, 25 deg C 2.) 12h, reflux

With tetrabutyl ammonium fluoride; sodium hydride; In tetrahydrofuran;
DOI:10.1021/jo00176a002

Reference yield:

: 82444-68-6
N-<3-<(tert-butylcarbonyl)oxy>cyclohex-2-enylidene>-N-<2-<(trimethylsilyl)methyl>-2-propenyl>methylammonium perchlorate

: 87883-84-9
3-cyclohex-2-enone

Guidance literature:: Multi-step reaction with 2 steps

1: CsF / acetonitrile / 24 h / 25 °C

2: 31 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 1.) 14h, 25 deg C 2.) 12h, reflux

With tetrabutyl ammonium fluoride; cesium fluoride; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jo00176a002