4H-1-Benzopyran-4-one, 6-chloro-5,8-dihydroxy-2-phenyl-

Base Information

Chemical Name:4H-1-Benzopyran-4-one, 6-chloro-5,8-dihydroxy-2-phenyl-
CAS No.:87953-84-2
Molecular Formula:C15H9ClO4
Molecular Weight:288.687
Hs Code.:

Synonyms:

Suppliers and Price of 4H-1-Benzopyran-4-one, 6-chloro-5,8-dihydroxy-2-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 3 raw suppliers

Chemical Property of 4H-1-Benzopyran-4-one, 6-chloro-5,8-dihydroxy-2-phenyl-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4H-1-Benzopyran-4-one, 6-chloro-5,8-dihydroxy-2-phenyl-

There total 9 articles about 4H-1-Benzopyran-4-one, 6-chloro-5,8-dihydroxy-2-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 87953-83-1
5,8-Quinoflavone

: 87953-84-2
6-chloro-5,8-dihydroxyflavone

Guidance literature:: With hydrogenchloride; In acetic acid; for 0.0583333h; Heating;
DOI:10.1021/jo00178a013

Reference yield:

: 87953-90-0
6-Chloro-5-hydroxyflavone

: 87953-84-2
6-chloro-5,8-dihydroxyflavone

Guidance literature:: With pyridine; dipotassium peroxodisulfate; tetraethylammonium hydroxide; In water; at 35 ℃; for 20h;
DOI:10.1021/jo00178a013

Reference yield:

: 703-23-1
2'-hydroxy-6'-methoxyacetophenone

: 87953-84-2
6-chloro-5,8-dihydroxyflavone

Guidance literature:: Multi-step reaction with 6 steps

1: 1.05 g / sulfuryl chloride / acetic acid / 1.5 h, 115 deg C, then reflux , 30 min

2: 87.4 percent / pyridine / 0.5 h / Heating

3: 71.5 percent / powdered sodium hydroxide / pyridine / 4 h / Ambient temperature

4: acetic acid / 4 h / Heating

5: 89.3 percent / conc. HCl / acetic acid / 4 h / Heating

6: 1.05 g / tetraethylammonium hydroxide, Py_., potassium peroxydisulfate, Py_. / H₂O / 20 h / 35 °C

With pyridine; hydrogenchloride; sodium hydroxide; dipotassium peroxodisulfate; sulfuryl dichloride; tetraethylammonium hydroxide; In pyridine; water; acetic acid;
DOI:10.1021/jo00178a013