4,4-Dimethyl-3,3,5,5-tetraphenyl-1,2,4-dithiagermolane

Base Information

• Chemical Name: 4,4-Dimethyl-3,3,5,5-tetraphenyl-1,2,4-dithiagermolane
• CAS No.: 87993-94-0
• Molecular Formula: C28H26GeS2
• Molecular Weight: 499.236
• DSSTox Substance ID: DTXSID10520981
• Wikidata: Q82385182

Synonyms:87993-94-0;4,4-Dimethyl-3,3,5,5-tetraphenyl-1,2,4-dithiagermolane;DTXSID10520981

Chemical Property of 4,4-Dimethyl-3,3,5,5-tetraphenyl-1,2,4-dithiagermolane

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 4
• Exact Mass: 500.0687709
• Heavy Atom Count: 31
• Complexity: 492

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C[Ge]1(C(SSC1(C2=CC=CC=C2)C3=CC=CC=C3)(C4=CC=CC=C4)C5=CC=CC=C5)C

Technology Process of 4,4-Dimethyl-3,3,5,5-tetraphenyl-1,2,4-dithiagermolane

There total 1 articles about 4,4-Dimethyl-3,3,5,5-tetraphenyl-1,2,4-dithiagermolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

(CH3)2Ge(C(C6H5)2I)2 (87993-92-8) → dimethyl-4,4 tetraphenyl-3,3,5,5 germa-4 dithiolane-1,2 (87993-94-0) + dimethyl-3,3 tetraphenyl-2,2,4,4 germa-3 thietane (87993-89-3)

Guidance literature:

With hydrogen sulfide; triethylamine; In pentane; byproducts: Et3N*HI;

DOI:10.1016/S0022-328X(00)99841-3

Reference yield: 90.0%

dimethyl-4,4 tetraphenyl-3,3,5,5 germa-4 dithiolane-1,2 (87993-94-0) → dimethyl-3,3 tetraphenyl-2,2,4,4 germa-3 thietane (87993-89-3)

Guidance literature:

With tris(triethylamino)phosphine; In not given; byproducts: (Et2N)3PS;

DOI:10.1016/S0022-328X(00)99841-3

upstream raw materials:

(CH₃)2Ge(C(C₆H₅)2I)2

Downstream raw materials:

dimethyl-3,3 tetraphenyl-2,2,4,4 germa-3 thietane

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