Technology Process of Hexadecanoic acid,
2-[[bis(phenylmethoxy)phosphinyl]oxy]-1-methylethyl ester, (R)-
There total 7 articles about Hexadecanoic acid,
2-[[bis(phenylmethoxy)phosphinyl]oxy]-1-methylethyl ester, (R)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 40 percent / CHCl3
2: 64 percent / Ca(NO3)2, (NH4)2SO4, 7500 IU of lipase / diethyl ether; methanol; H2O / Ambient temperature
3: 1.) methyltriphenoxyphosphonium iodide, 2.) tetrabutylammonium borohydride / 1.) CH2Cl2, room temperature, 2.) HMPA, room temperature
With
ammonium sulfate; 7500 IU of lipase; calcium(II) nitrate; methyltriphenoxyphosphonium iodide; tetrabutylammonium borohydride;
In
methanol; diethyl ether; chloroform; water;
DOI:10.1021/ja00315a049
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 40 percent / CHCl3
2: 64 percent / Ca(NO3)2, (NH4)2SO4, 7500 IU of lipase / diethyl ether; methanol; H2O / Ambient temperature
3: 1.) methyltriphenoxyphosphonium iodide, 2.) tetrabutylammonium borohydride / 1.) CH2Cl2, room temperature, 2.) HMPA, room temperature
With
ammonium sulfate; 7500 IU of lipase; calcium(II) nitrate; methyltriphenoxyphosphonium iodide; tetrabutylammonium borohydride;
In
methanol; diethyl ether; chloroform; water;
DOI:10.1021/ja00315a049
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 10 percent / CHCl3; diethyl ether / 96 h / Ambient temperature
2: 64 percent / Ca(NO3)2, (NH4)2SO4, 7500 IU of lipase / diethyl ether; methanol; H2O / Ambient temperature
3: 1.) methyltriphenoxyphosphonium iodide, 2.) tetrabutylammonium borohydride / 1.) CH2Cl2, room temperature, 2.) HMPA, room temperature
With
ammonium sulfate; 7500 IU of lipase; calcium(II) nitrate; methyltriphenoxyphosphonium iodide; tetrabutylammonium borohydride;
In
methanol; diethyl ether; chloroform; water;
DOI:10.1021/ja00315a049