3,4-Bis[(4-chlorophenyl)methoxy]benzaldehyde

Base Information

Chemical Name:3,4-Bis[(4-chlorophenyl)methoxy]benzaldehyde
CAS No.:88036-81-1
Molecular Formula:C21H16Cl2O3
Molecular Weight:387.262
Hs Code.:
DSSTox Substance ID:DTXSID20595529
Wikidata:Q82490545

Synonyms:3,4-Bis[(4-chlorophenyl)methoxy]benzaldehyde;88036-81-1;SCHEMBL7149581;DTXSID20595529

Suppliers and Price of 3,4-Bis[(4-chlorophenyl)methoxy]benzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,4-Bis[(4-chlorophenyl)methoxy]benzaldehyde

Chemical Property:

XLogP3:5.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:7
Exact Mass:386.0476498
Heavy Atom Count:26
Complexity:418

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1COC2=C(C=C(C=C2)C=O)OCC3=CC=C(C=C3)Cl)Cl

Technology Process of 3,4-Bis[(4-chlorophenyl)methoxy]benzaldehyde

There total 3 articles about 3,4-Bis[(4-chlorophenyl)methoxy]benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 873-76-7
para-Chlorobenzyl alcohol

: 383423-79-8
4-(4-chloro-benzyloxy)-3-hydroxy-benzaldehyde

: 88036-81-1
3,4-bis-(4-chlorophenyl-methoxy)-benzaldehyde

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 23 ℃; for 5h;
DOI:10.1002/1521-3765(20010903)7:17<3798::AID-CHEM3798>3.0.CO;2-6

Reference yield:

: 622-95-7
4-chlorobenzyl bromide

: 88036-81-1
3,4-bis-(4-chlorophenyl-methoxy)-benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaH / dimethylformamide / 0.17 h / 0 °C

1.2: dimethylformamide / 12 h / 0 - 23 °C

2.1: PPh₃; DEAD / tetrahydrofuran / 5 h / 23 °C

With sodium hydride; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; N,N-dimethyl-formamide; 2.1: Mitsunobu reaction;
DOI:10.1002/1521-3765(20010903)7:17<3798::AID-CHEM3798>3.0.CO;2-6

Reference yield:

: 139-85-5
3,4-dihydroxybenzaldehyde

: 88036-81-1
3,4-bis-(4-chlorophenyl-methoxy)-benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaH / dimethylformamide / 0.17 h / 0 °C

1.2: dimethylformamide / 12 h / 0 - 23 °C

2.1: PPh₃; DEAD / tetrahydrofuran / 5 h / 23 °C

With sodium hydride; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; N,N-dimethyl-formamide; 2.1: Mitsunobu reaction;
DOI:10.1002/1521-3765(20010903)7:17<3798::AID-CHEM3798>3.0.CO;2-6