2-Chloro-3-hydroxy-6-nitro-4-(prop-2-en-1-yl)benzaldehyde

Base Information

Chemical Name:2-Chloro-3-hydroxy-6-nitro-4-(prop-2-en-1-yl)benzaldehyde
CAS No.:88062-17-3
Molecular Formula:C₁₀H₈ClNO₄
Molecular Weight:241.631
Hs Code.:
DSSTox Substance ID:DTXSID20521949
Wikidata:Q82386813

Synonyms:88062-17-3;DTXSID20521949;2-Chloro-3-hydroxy-6-nitro-4-(prop-2-en-1-yl)benzaldehyde

Suppliers and Price of 2-Chloro-3-hydroxy-6-nitro-4-(prop-2-en-1-yl)benzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Chloro-3-hydroxy-6-nitro-4-(prop-2-en-1-yl)benzaldehyde

Chemical Property:

XLogP3:2.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:241.0141854
Heavy Atom Count:16
Complexity:291

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=CCC1=CC(=C(C(=C1O)Cl)C=O)[N+](=O)[O-]

Technology Process of 2-Chloro-3-hydroxy-6-nitro-4-(prop-2-en-1-yl)benzaldehyde

There total 2 articles about 2-Chloro-3-hydroxy-6-nitro-4-(prop-2-en-1-yl)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 344559-44-0
3-Allyloxy-2-chloro-6-nitro-benzaldehyde

: 88062-17-3
2-chloro-3-hydroxy-6-nitro-4-propenylbenzaldehyde

Guidance literature:: In diphenylether; at 225 - 230 ℃; for 1h;
DOI:10.1002/jhet.5570200443

Reference yield:

: 19183-03-0
2-chloro-6-nitro-3-hydroxybenzaldehyde

: 88062-17-3
2-chloro-3-hydroxy-6-nitro-4-propenylbenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / K₂CO₃ / dimethylformamide / 6 h / 60 °C

2: 47 percent / diphenyl ether / 1 h / 225 - 230 °C

With potassium carbonate; In diphenylether; N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570200443

Reference yield:

: 88062-17-3
2-chloro-3-hydroxy-6-nitro-4-propenylbenzaldehyde

: 88062-23-1
8-chloro-3,5-dihydro-5-phenyl-2H-furo<2,3-f>indole-2-methanol

Guidance literature:: Multi-step reaction with 5 steps

1: 64 percent / 85percent m-chloroperoxybenzoic acid / CH₂Cl₂ / 20 h / Ambient temperature

2: 1) NaOH; 2) CH₃COONa / 1) methanol, water, THF, 10 deg C, 1 h; 2) 140 deg C, 30 min.

3: 85 percent / Fe powder / ethanol; acetic acid / 0.42 h

4: 99 percent / K₂CO₃ / methanol / 0.58 h / Ambient temperature

5: 58 percent / Cu₂Br₂, Na₂CO₃ / various solvent(s) / 3 h / 170 °C

With copper(I) bromide; sodium hydroxide; sodium acetate; iron; sodium carbonate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In methanol; ethanol; dichloromethane; acetic acid;
DOI:10.1002/jhet.5570200443