2-[(2,3-Dichloro-4-methoxyphenyl)sulfanyl]propan-1-ol

Base Information

Chemical Name:2-[(2,3-Dichloro-4-methoxyphenyl)sulfanyl]propan-1-ol
CAS No.:88062-52-6
Molecular Formula:C10H12Cl2O2S
Molecular Weight:267.176
Hs Code.:
DSSTox Substance ID:DTXSID90579351

Synonyms:88062-52-6;2-[(2,3-Dichloro-4-methoxyphenyl)sulfanyl]propan-1-ol;DTXSID90579351

Suppliers and Price of 2-[(2,3-Dichloro-4-methoxyphenyl)sulfanyl]propan-1-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[(2,3-Dichloro-4-methoxyphenyl)sulfanyl]propan-1-ol

Chemical Property:

XLogP3:3.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:265.9935062
Heavy Atom Count:15
Complexity:194

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(CO)SC1=C(C(=C(C=C1)OC)Cl)Cl

Technology Process of 2-[(2,3-Dichloro-4-methoxyphenyl)sulfanyl]propan-1-ol

There total 4 articles about 2-[(2,3-Dichloro-4-methoxyphenyl)sulfanyl]propan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 83119-56-6
α-<(2,3-dichloro-4-methoxy)phenylthio>propionic acid

: 88062-52-6
2-<(2,3-dichloro-4-methoxy)phenylthio>propanol

Guidance literature:: With borane; In tetrahydrofuran; for 1h; Heating;
DOI:10.1002/jhet.5570200406

Reference yield:

: 1984-59-4
2,3-dichloroanisole

: 88062-52-6
2-<(2,3-dichloro-4-methoxy)phenylthio>propanol

Guidance literature:: Multi-step reaction with 4 steps

1: 83 percent / chlorosulfonic acid / 1 h / Ambient temperature

2: 88 percent / conc. sulfuric acid, zinc dust / H₂O / 16 h / Heating

3: 1) sodium hydride; 2) 3N HCl / 1) DMF, 10 min; 2) room temp., 3 h

4: 74 percent / 1.0 M borane / tetrahydrofuran / 1 h / Heating

With hydrogenchloride; chlorosulfonic acid; sulfuric acid; borane; sodium hydride; zinc; In tetrahydrofuran; water;
DOI:10.1002/jhet.5570200406

Reference yield:

: 35509-60-5
2,3-dichloro-4-methoxybenzenesulfonyl chloride

: 88062-52-6
2-<(2,3-dichloro-4-methoxy)phenylthio>propanol

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / conc. sulfuric acid, zinc dust / H₂O / 16 h / Heating

2: 1) sodium hydride; 2) 3N HCl / 1) DMF, 10 min; 2) room temp., 3 h

3: 74 percent / 1.0 M borane / tetrahydrofuran / 1 h / Heating

With hydrogenchloride; sulfuric acid; borane; sodium hydride; zinc; In tetrahydrofuran; water;
DOI:10.1002/jhet.5570200406