(1R,2R)-2-[(2,3-Dichloro-4-methoxyphenyl)sulfanyl]cyclohexan-1-ol

Base Information

Chemical Name:(1R,2R)-2-[(2,3-Dichloro-4-methoxyphenyl)sulfanyl]cyclohexan-1-ol
CAS No.:88062-56-0
Molecular Formula:C₁₃H₁₆Cl₂O₂S
Molecular Weight:307.241
Hs Code.:
DSSTox Substance ID:DTXSID10579353
Wikidata:Q82469848

Synonyms:88062-56-0;DTXSID10579353;(1R,2R)-2-[(2,3-Dichloro-4-methoxyphenyl)sulfanyl]cyclohexan-1-ol

Suppliers and Price of (1R,2R)-2-[(2,3-Dichloro-4-methoxyphenyl)sulfanyl]cyclohexan-1-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of (1R,2R)-2-[(2,3-Dichloro-4-methoxyphenyl)sulfanyl]cyclohexan-1-ol

Chemical Property:

XLogP3:4.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:306.0248063
Heavy Atom Count:18
Complexity:267

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C(=C(C=C1)SC2CCCCC2O)Cl)Cl
Isomeric SMILES:COC1=C(C(=C(C=C1)S[C@@H]2CCCC[C@H]2O)Cl)Cl

Technology Process of (1R,2R)-2-[(2,3-Dichloro-4-methoxyphenyl)sulfanyl]cyclohexan-1-ol

There total 3 articles about (1R,2R)-2-[(2,3-Dichloro-4-methoxyphenyl)sulfanyl]cyclohexan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1984-59-4
2,3-dichloroanisole

: 88062-56-0
trans-2-<(2,3-dichloro-4-methoxy)phenylthio>cyclohexanol

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / chlorosulfonic acid / 1 h / Ambient temperature

2: 88 percent / conc. sulfuric acid, zinc dust / H₂O / 16 h / Heating

3: sodium hydride / 1) DMF, hexane, 30 min; 2) DMF, room tepm., overnight

With chlorosulfonic acid; sulfuric acid; sodium hydride; zinc; In water;
DOI:10.1002/jhet.5570200406

Reference yield:

: 35509-60-5
2,3-dichloro-4-methoxybenzenesulfonyl chloride

: 88062-56-0
trans-2-<(2,3-dichloro-4-methoxy)phenylthio>cyclohexanol

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / conc. sulfuric acid, zinc dust / H₂O / 16 h / Heating

2: sodium hydride / 1) DMF, hexane, 30 min; 2) DMF, room tepm., overnight

With sulfuric acid; sodium hydride; zinc; In water;
DOI:10.1002/jhet.5570200406

Reference yield:

: 286-20-4
cyclohexane-1,2-epoxide

: 83119-51-1
2,3-dichloro-4-methoxythiophenol

: 88062-56-0
trans-2-<(2,3-dichloro-4-methoxy)phenylthio>cyclohexanol

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1) DMF, hexane, 30 min; 2) DMF, room tepm., overnight;
DOI:10.1002/jhet.5570200406