5-Methyl-1-phenylhex-5-en-3-one

Base Information

Chemical Name:5-Methyl-1-phenylhex-5-en-3-one
CAS No.:88068-36-4
Molecular Formula:C13H16O
Molecular Weight:188.269
Hs Code.:
DSSTox Substance ID:DTXSID10521236
Wikidata:Q82385601

Synonyms:5-Methyl-1-phenylhex-5-en-3-one;88068-36-4;DTXSID10521236;AKOS017729875

Suppliers and Price of 5-Methyl-1-phenylhex-5-en-3-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-Methyl-1-phenylhex-5-en-3-one

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:5
Exact Mass:188.120115130
Heavy Atom Count:14
Complexity:199

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=C)CC(=O)CCC1=CC=CC=C1

Technology Process of 5-Methyl-1-phenylhex-5-en-3-one

There total 4 articles about 5-Methyl-1-phenylhex-5-en-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 115413-92-8,84212-92-0
5-methyl-1-phenyl-5-hexen-3-ol

: 88068-36-4
2-methyl-4-oxo-6-phenyl-1-hexene

Guidance literature:: With Jones reagent; In acetone; at 0 - 20 ℃; for 1h;
DOI:10.1002/ejoc.201600998

Reference yield:

: 104-53-0
3-phenyl-propionaldehyde

: 88068-36-4
2-methyl-4-oxo-6-phenyl-1-hexene

Guidance literature:: Multi-step reaction with 2 steps

1: indium / tetrahydrofuran; water / 24 h / 20 °C

2: Jones reagent / acetone / 1 h / 0 - 20 °C

With indium; Jones reagent; In tetrahydrofuran; water; acetone; 2: |Jones Oxidation;
DOI:10.1002/ejoc.201600998

Reference yield:

: (3-Benzenesulfonyl-3-methyl-1-phenethyl-cyclobutoxy)-trimethyl-silane

: 88068-36-4
2-methyl-4-oxo-6-phenyl-1-hexene

Guidance literature:: Multi-step reaction with 2 steps

1: 1 M HCl / ethanol / 0.5 h / Ambient temperature

2: potassium hydride / tetrahydrofuran / 0.08 h / Ambient temperature

With hydrogenchloride; potassium hydride; In tetrahydrofuran; ethanol;
DOI:10.1246/cl.1983.1285