1-(9-Acetyl-9H-carbazol-2-yl)-2-(triphenyl-lambda~5~-phosphanylidene)ethan-1-one

Base Information

Chemical Name:1-(9-Acetyl-9H-carbazol-2-yl)-2-(triphenyl-lambda~5~-phosphanylidene)ethan-1-one
CAS No.:88092-99-3
Molecular Formula:C₃₄H₂₆NO₂P
Molecular Weight:511.56
Hs Code.:
DSSTox Substance ID:DTXSID60520931
Wikidata:Q82385110

Synonyms:88092-99-3;DTXSID60520931;1-(9-Acetyl-9H-carbazol-2-yl)-2-(triphenyl-lambda~5~-phosphanylidene)ethan-1-one

Suppliers and Price of 1-(9-Acetyl-9H-carbazol-2-yl)-2-(triphenyl-lambda~5~-phosphanylidene)ethan-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(9-Acetyl-9H-carbazol-2-yl)-2-(triphenyl-lambda~5~-phosphanylidene)ethan-1-one

Chemical Property:

XLogP3:6.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:511.17011607
Heavy Atom Count:38
Complexity:842

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=O)N1C2=CC=CC=C2C3=C1C=C(C=C3)C(=O)C=P(C4=CC=CC=C4)(C5=CC=CC=C5)C6=CC=CC=C6

Technology Process of 1-(9-Acetyl-9H-carbazol-2-yl)-2-(triphenyl-lambda~5~-phosphanylidene)ethan-1-one

There total 3 articles about 1-(9-Acetyl-9H-carbazol-2-yl)-2-(triphenyl-lambda~5~-phosphanylidene)ethan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: <<(9-acetylcarbazol-2-yl)carbonyl>methyl>triphenylphosphonium chloride

: 88092-99-3,88093-12-3
<<(fluoren-2-yl)carbonyl>methylene>triphenylphosphorane

Guidance literature:: With sodium ethanolate; In ethanol; for 0.5h;

Reference yield:

: 574-39-0
9-acetylcarbazole

: 88092-99-3,88093-12-3
<<(fluoren-2-yl)carbonyl>methylene>triphenylphosphorane

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / AlCl₃ / 1,2-dichloro-ethane / 6.5 h / Ambient temperature

2: 90 percent / fusion

3: 92 percent / NaOEt / ethanol / 0.5 h

With aluminium trichloride; sodium ethanolate; In ethanol; 1,2-dichloro-ethane;

Reference yield:

: 88092-92-6
9-acetyl-2-(chloroacetyl)carbazole

: 88092-99-3,88093-12-3
<<(fluoren-2-yl)carbonyl>methylene>triphenylphosphorane

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / fusion

2: 92 percent / NaOEt / ethanol / 0.5 h

With sodium ethanolate; In ethanol;