N-(3,3-Diethoxypropyl)-N-phenylmethanesulfonamide

Base Information

Chemical Name:N-(3,3-Diethoxypropyl)-N-phenylmethanesulfonamide
CAS No.:88131-56-0
Molecular Formula:C14H23NO4S
Molecular Weight:301.407
Hs Code.:
DSSTox Substance ID:DTXSID40530199
Wikidata:Q82401185

Synonyms:88131-56-0;N-(3,3-Diethoxypropyl)-N-phenylmethanesulfonamide;DTXSID40530199

Suppliers and Price of N-(3,3-Diethoxypropyl)-N-phenylmethanesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of N-(3,3-Diethoxypropyl)-N-phenylmethanesulfonamide

Chemical Property:

XLogP3:2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:9
Exact Mass:301.13477939
Heavy Atom Count:20
Complexity:341

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(CCN(C1=CC=CC=C1)S(=O)(=O)C)OCC

Technology Process of N-(3,3-Diethoxypropyl)-N-phenylmethanesulfonamide

There total 2 articles about N-(3,3-Diethoxypropyl)-N-phenylmethanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 59067-07-1
3-bromopropinaldehyde diethyl acetal

: 1197-22-4
N-phenylmethanesulfonamide

: 88131-56-0
N-(3,3-Diethoxy-propyl)-N-phenyl-methanesulfonamide

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 110 ℃;
DOI:10.1021/jo00176a007

Reference yield:

: 62-53-3
aniline

: 88131-56-0
N-(3,3-Diethoxy-propyl)-N-phenyl-methanesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / CH₂Cl₂ / 1) 1 h, 0 deg C; 2) 1 h, 25 deg C

2: 61 percent / NaH / dimethylformamide / 110 °C

With pyridine; sodium hydride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00176a007

Reference yield:

: 88131-56-0
N-(3,3-Diethoxy-propyl)-N-phenyl-methanesulfonamide

: 30831-92-6
1-(methylsulfonyl)-1,2-dihydroquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / TiCl₄ / toluene / 0 °C

2: 91 percent / 160 °C

With titanium tetrachloride; In toluene;
DOI:10.1021/jo00176a007