N-[4-(3,4-dimethoxyphenyl)-2-oxocyclohex-3-en-1-yl]acetamide

Base Information

Chemical Name:N-[4-(3,4-dimethoxyphenyl)-2-oxocyclohex-3-en-1-yl]acetamide
CAS No.:88141-45-1
Molecular Formula:C16H19NO4
Molecular Weight:289.331
Hs Code.:
DSSTox Substance ID:DTXSID70521919

Synonyms:88141-45-1;DTXSID70521919;N-(3',4'-Dimethoxy-5-oxo[2,3,4,5-tetrahydro[1,1'-biphenyl]]-4-yl)acetamide

Suppliers and Price of N-[4-(3,4-dimethoxyphenyl)-2-oxocyclohex-3-en-1-yl]acetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
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Total 0 raw suppliers

Chemical Property of N-[4-(3,4-dimethoxyphenyl)-2-oxocyclohex-3-en-1-yl]acetamide

Chemical Property:

XLogP3:1.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:289.13140809
Heavy Atom Count:21
Complexity:432

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)NC1CCC(=CC1=O)C2=CC(=C(C=C2)OC)OC

Technology Process of N-[4-(3,4-dimethoxyphenyl)-2-oxocyclohex-3-en-1-yl]acetamide

There total 2 articles about N-[4-(3,4-dimethoxyphenyl)-2-oxocyclohex-3-en-1-yl]acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20036-53-7
3-<3,4-(dimethoxy)phenyl>-2-cyclohexen-1-one

: 88141-45-1
N-[4-(3,4-Dimethoxy-phenyl)-2-oxo-cyclohex-3-enyl]-acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / NH₂OH*HCl, K₂CO₃ / ethanol; H₂O / 1 h / Heating

2: 69 percent / pyridine / 1.) 1 h, ice cooling, 2.) 30 min, r.t.

With pyridine; hydroxylamine hydrochloride; potassium carbonate; In ethanol; water;
DOI:10.1248/cpb.31.2016

Reference yield:

: 88141-38-2
3-(3,4-dimethoxy)cyclohex-2-enone oxime

: 88141-45-1
N-[4-(3,4-Dimethoxy-phenyl)-2-oxo-cyclohex-3-enyl]-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / pyridine / 1.) 1 h, ice cooling, 2.) 30 min, r.t.

With pyridine;
DOI:10.1248/cpb.31.2016