Phosphonic acid, 1-piperidinyl-, disodium salt

Base Information

• Chemical Name: Phosphonic acid, 1-piperidinyl-, disodium salt
• CAS No.: 117018-90-3
• Molecular Formula: C₅H₁₀NO₃P*2Na
• Molecular Weight: 209.093
• DSSTox Substance ID: DTXSID70151674
• Nikkaji Number: J1.741.909I
• Mol file: 117018-90-3.mol

Synonyms:1-Piperidinylphosphonic acid disodium salt;Phosphonic acid, 1-piperidinyl-, disodium salt;117018-90-3;C5H12NO3P.2Na;DTXSID70151674;C5-H12-N-O3-P.2Na;Piperidinophosphonic acid disodium salt;LS-106768

Chemical Property of Phosphonic acid, 1-piperidinyl-, disodium salt

Chemical Property:

• Vapor Pressure: 2.4E-05mmHg at 25°C
• Boiling Point: 334.7°Cat760mmHg
• Flash Point: 156.2°C
• Density: g/cm³
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 0
• Exact Mass: 209.01936874
• Heavy Atom Count: 12
• Complexity: 138

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CCN(CC1)P(=O)([O-])[O-].[Na+].[Na+]

Technology Process of Phosphonic acid, 1-piperidinyl-, disodium salt

There total 2 articles about Phosphonic acid, 1-piperidinyl-, disodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

Bis(trimethylsilyl) piperididophosphate (117018-87-8) → C5H10NO3P(2-)*2Na(1+) (117018-90-3)

Guidance literature:

With sodium; In methanol; at 5 - 10 ℃;

DOI:10.1007/BF00763381

Reference yield:

Dimethyl piperididophosphate (597-24-0) → C5H10NO3P(2-)*2Na(1+) (117018-90-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 81 percent / CH₂Cl₂ / 24 h / 20 °C

2: 95 percent / Na / methanol / 5 - 10 °C

With sodium; In methanol; dichloromethane;

DOI:10.1007/BF00763381

upstream raw materials:

Bis(trimethylsilyl) piperididophosphate

Dimethyl piperididophosphate