Fluorenyl, 1,2,3,4,5,7,8-heptachloro-6-methoxy-9-(pentachlorophenyl)-

Base Information

• Chemical Name: Fluorenyl, 1,2,3,4,5,7,8-heptachloro-6-methoxy-9-(pentachlorophenyl)-
• CAS No.: 88180-09-0
• Molecular Formula: C20H3Cl12O
• Molecular Weight: 684.679
• Mol file: 88180-09-0.mol

Synonyms:

Chemical Property of Fluorenyl, 1,2,3,4,5,7,8-heptachloro-6-methoxy-9-(pentachlorophenyl)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Fluorenyl, 1,2,3,4,5,7,8-heptachloro-6-methoxy-9-(pentachlorophenyl)-

There total 1 articles about Fluorenyl, 1,2,3,4,5,7,8-heptachloro-6-methoxy-9-(pentachlorophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

9H-Dodecachloro-9-phenylfluoren-3-ol (88180-10-3) → 3-Methoxydodecachloro-9-phenylfluorenyl radical (88180-09-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 93 percent / diethyl ether; CHCl₃

2: 1.) NaOH; 2.) I₂ / 1.) diethyl ether, DMSO, 3 min; 2.) 15 min

With sodium hydroxide; iodine; In diethyl ether; chloroform;

DOI:10.1021/jo00179a007

Reference yield: 90.0%

3-Methoxydodecachloro-9-phenylfluorenyl radical (88180-09-0) → perchloro(9-phenyl-3-fluorenone) (88180-07-8)

Guidance literature:

With antimonypentachloride; In dichloromethane;

DOI:10.1021/jo00179a007

upstream raw materials:

9H-Dodecachloro-9-phenylfluoren-3-ol

Downstream raw materials:

perchloro(9-phenyl-3-fluorenone)