1,2,4,5-Benzenetetrol, 3-chloro-6-methyl-, tetraacetate

Base Information

Chemical Name:1,2,4,5-Benzenetetrol, 3-chloro-6-methyl-, tetraacetate
CAS No.:88207-75-4
Molecular Formula:C₁₅H₁₅ClO₈
Molecular Weight:358.732
Hs Code.:

Synonyms:

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Chemical Property of 1,2,4,5-Benzenetetrol, 3-chloro-6-methyl-, tetraacetate

Chemical Property:

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Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of 1,2,4,5-Benzenetetrol, 3-chloro-6-methyl-, tetraacetate

There total 7 articles about 1,2,4,5-Benzenetetrol, 3-chloro-6-methyl-, tetraacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 504-15-4
orcinol

: 88207-75-4
2,3,5,6-tetraacetoxy-4-chloro-toluene

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / sulphuryl chloride / acetic acid / 3 h / Ambient temperature

2: 83 percent / Fremy's salt, K₂HPO₄ / H₂O / 24 h / Ambient temperature

3: 39 percent / NaOH / H₂O / 2 h / Heating

4: 1.) H₂, 2.) NaOAc / 1.) 10percent Pd-carbon / 1.) ethyl acetate, 1 h, 2.) 100 deg C, 15 min

With sodium hydroxide; dipotassium hydrogenphosphate; sulfuryl dichloride; potassiuim nitrosodisulfonate; hydrogen; sodium acetate; palladium on activated charcoal; In water; acetic acid;

Reference yield:

: 27808-83-9
ethyl 3,5-dichloro-2,4-dihydroxy-6-methylbenzoate

: 88207-75-4
2,3,5,6-tetraacetoxy-4-chloro-toluene

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) aq. NaOH / 1.) H₂O, reflux, 3 h, 2.) benzene, animal charcoal, reflux, 1 h

2: Fremy's salt, K₂HPO₄ / H₂O / 24 h / Ambient temperature

3: 39 percent / NaOH / H₂O / 2 h / Heating

4: 1.) H₂, 2.) NaOAc / 1.) 10percent Pd-carbon / 1.) ethyl acetate, 1 h, 2.) 100 deg C, 15 min

With sodium hydroxide; dipotassium hydrogenphosphate; potassiuim nitrosodisulfonate; hydrogen; sodium acetate; palladium on activated charcoal; In water;

Reference yield:

: 88207-72-1
2,4-dichloro-5-methyl-resorcinol

: 88207-75-4
2,3,5,6-tetraacetoxy-4-chloro-toluene

Guidance literature:: Multi-step reaction with 3 steps

1: Fremy's salt, K₂HPO₄ / H₂O / 24 h / Ambient temperature

2: 39 percent / NaOH / H₂O / 2 h / Heating

3: 1.) H₂, 2.) NaOAc / 1.) 10percent Pd-carbon / 1.) ethyl acetate, 1 h, 2.) 100 deg C, 15 min

With sodium hydroxide; dipotassium hydrogenphosphate; potassiuim nitrosodisulfonate; hydrogen; sodium acetate; palladium on activated charcoal; In water;