4-cyclohexylhexanoic acid

Base Information

Chemical Name:4-cyclohexylhexanoic acid
CAS No.:6293-41-0
Molecular Formula:C12H22O2
Molecular Weight:198.3019
Hs Code.:

Synonyms:

Suppliers and Price of 4-cyclohexylhexanoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of 4-cyclohexylhexanoic acid

Chemical Property:

Vapor Pressure:0.000134mmHg at 25°C
Boiling Point:310.3°Cat760mmHg
Flash Point:148.2°C
Density:0.978g/cm³

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-cyclohexylhexanoic acid

There total 7 articles about 4-cyclohexylhexanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 592509-72-3
4-cyclohexyl-hexanoic acid ethyl ester

: 6293-41-0
4-cyclohexyl-hexanoic acid

Guidance literature:: With lithium hydroxide; water; In tetrahydrofuran; ethanol; at 20 ℃;
DOI:10.1021/jo0347011

Reference yield:

: 33856-70-1
2-Cyclohexyl-butanal

: 6293-41-0
4-cyclohexyl-hexanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / toluene / Heating

2: 74 percent / H₂ / Pd/C / methanol / 20 °C

3: 95 percent / LiOH*H₂O; H₂O / tetrahydrofuran; ethanol / 20 °C

With lithium hydroxide; water; hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; toluene;
DOI:10.1021/jo0347011

Reference yield:

: 14352-61-5
methyl cyclohexylacetate

: 6293-41-0
4-cyclohexyl-hexanoic acid

Guidance literature:: Multi-step reaction with 6 steps

1.1: LDA; 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone / tetrahydrofuran; hexane / 1 h / -78 °C

1.2: 95 percent / tetrahydrofuran; hexane / 14 h / -78 - 20 °C

2.1: 83 percent / diisobutylaluminum hydride / CH₂Cl₂; toluene / 0 - 20 °C

3.1: 81 percent / PDC; celite / CH₂Cl₂ / 1 h / 20 °C

4.1: 88 percent / toluene / Heating

5.1: 74 percent / H₂ / Pd/C / methanol / 20 °C

6.1: 95 percent / LiOH*H₂O; H₂O / tetrahydrofuran; ethanol / 20 °C

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; lithium hydroxide; dipyridinium dichromate; Celite; water; hydrogen; diisobutylaluminium hydride; lithium diisopropyl amide; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; toluene;
DOI:10.1021/jo0347011