Methanol, methoxy(5-methyl-2-phenyl-4(5H)-oxazolylidene)-, lithium salt, (R)-

Base Information

Chemical Name:Methanol, methoxy(5-methyl-2-phenyl-4(5H)-oxazolylidene)-, lithium salt, (R)-
CAS No.:88318-67-6
Molecular Formula:C₁₂H₁₂NO₃*Li
Molecular Weight:225.173
Hs Code.:

Synonyms:

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Chemical Property of Methanol, methoxy(5-methyl-2-phenyl-4(5H)-oxazolylidene)-, lithium salt, (R)-

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Technology Process of Methanol, methoxy(5-methyl-2-phenyl-4(5H)-oxazolylidene)-, lithium salt, (R)-

There total 4 articles about Methanol, methoxy(5-methyl-2-phenyl-4(5H)-oxazolylidene)-, lithium salt, (R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60538-17-2,62107-40-8,74272-77-8,79952-14-0,79952-15-1,82659-84-5,88336-08-7
(4S,5R)-4-methyl-2-phenyl-4,5-dihydrooxazole-4-carboxylic acid methyl ester

: 88318-67-6,88318-68-7
Lithium; methoxy-[(R)-5-methyl-2-phenyl-oxazol-(4E)-ylidene]-methanolate

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; at -75 ℃;
DOI:10.1016/S0040-4039(00)86256-5

Reference yield:

: 82659-84-5
(4S,5S)-5-methyl-2-phenyl-4,5-dihydro-oxazole-4-carboxylic acid methyl ester

: 88318-67-6,88318-68-7
Lithium; methoxy-[(S)-5-methyl-2-phenyl-oxazol-(4E)-ylidene]-methanolate

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; at -75 ℃;
DOI:10.1016/S0040-4039(00)86256-5

Reference yield:

: 79893-89-3
N-benzoyl-L-threonine methyl ester

: 88318-67-6,88318-68-7
Lithium; methoxy-[(S)-5-methyl-2-phenyl-oxazol-(4E)-ylidene]-methanolate

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / SOCl₂ / 98.4percent ds

2: LDA / tetrahydrofuran / -75 °C

With thionyl chloride; lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)86256-5