1-(3,3,3-Triethoxyprop-1-yn-1-yl)cyclohexan-1-ol

Base Information

Chemical Name:1-(3,3,3-Triethoxyprop-1-yn-1-yl)cyclohexan-1-ol
CAS No.:88329-64-0
Molecular Formula:C15H26O4
Molecular Weight:270.369
Hs Code.:
DSSTox Substance ID:DTXSID80528010
Wikidata:Q82397299

Synonyms:88329-64-0;1-(3,3,3-Triethoxyprop-1-yn-1-yl)cyclohexan-1-ol;DTXSID80528010;AKOS015906318;1-(3,3,3-triethoxy-1-propynyl)cyclohexanol;1-(3,3,3-triethoxy-prop-1-ynyl)-cyclohexan-1-ol

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(3,3,3-Triethoxyprop-1-yn-1-yl)cyclohexan-1-ol

Chemical Property:

XLogP3:1.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:8
Exact Mass:270.18310931
Heavy Atom Count:19
Complexity:303

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(C#CC1(CCCCC1)O)(OCC)OCC

Technology Process of 1-(3,3,3-Triethoxyprop-1-yn-1-yl)cyclohexan-1-ol

There total 4 articles about 1-(3,3,3-Triethoxyprop-1-yn-1-yl)cyclohexan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 91034-26-3
lithium ethyl orthopropiolate

: 88329-64-0
1-Triethoxyprop-1-ynyl-cyclohexanol

Guidance literature:: With n-butyllithium; In tetrahydrofuran; at 0 - 25 ℃; for 1h;
DOI:10.1016/S0040-4039(01)80072-1

Reference yield:

: triethoxycarbenium tetrafluoroborate

: 88329-64-0
1-Triethoxyprop-1-ynyl-cyclohexanol

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / n-BuLi / diethyl ether / -78 - 25 °C

2: n-BuLi / diethyl ether / 1 h / 0 °C

3: 89 percent / n-BuLi / tetrahydrofuran / 1 h / 0 - 25 °C

With n-butyllithium; In tetrahydrofuran; diethyl ether;
DOI:10.1016/S0040-4039(01)80072-1

Reference yield:

: 91022-26-3
trimethyl(3,3,3-triethoxyprop-1-yn-1-yl)silane

: 88329-64-0
1-Triethoxyprop-1-ynyl-cyclohexanol

Guidance literature:: Multi-step reaction with 2 steps

1: n-BuLi / diethyl ether / 1 h / 0 °C

2: 89 percent / n-BuLi / tetrahydrofuran / 1 h / 0 - 25 °C

With n-butyllithium; In tetrahydrofuran; diethyl ether;
DOI:10.1016/S0040-4039(01)80072-1