2-(6-Phenylhexyl)thiophene

Base Information

Chemical Name:2-(6-Phenylhexyl)thiophene
CAS No.:88336-89-4
Molecular Formula:C16H20S
Molecular Weight:244.401
Hs Code.:
DSSTox Substance ID:DTXSID201311880

Synonyms:2-(6-phenylhexyl)thiophene;DTXSID201311880;88336-89-4

Suppliers and Price of 2-(6-Phenylhexyl)thiophene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(6-Phenylhexyl)thiophene

Chemical Property:

XLogP3:5.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:7
Exact Mass:244.12857181
Heavy Atom Count:17
Complexity:184

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)CCCCCCC2=CC=CS2

Technology Process of 2-(6-Phenylhexyl)thiophene

There total 3 articles about 2-(6-Phenylhexyl)thiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 88343-63-9
2-(6-phenyl-1-oxohexyl)thiophene

: 88336-89-4
2-(6-Phenylhexyl)thiophene

Guidance literature:: With potassium hydroxide; hydrazine hydrate; In diethylene glycol; for 4h; Heating;
DOI:10.1021/jm00369a027

Reference yield:

: 21389-46-8
6-phenylhexanoyl chloride

: 88336-89-4
2-(6-Phenylhexyl)thiophene

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / SnCl₄ / CH₂Cl₂ / 2.5 h / 0 - 20 °C

2: 82 percent / NH₂NH₂*H₂O, KOH / bis-(2-hydroxy-ethyl) ether / 4 h / Heating

With potassium hydroxide; tin(IV) chloride; hydrazine hydrate; In dichloromethane; diethylene glycol;
DOI:10.1021/jm00369a027

Reference yield:

: 5581-75-9
6-phenylhexanic acid

: 88336-89-4
2-(6-Phenylhexyl)thiophene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) SOCl₂, 2.) SnCl₄ / 1.) 40 deg C, half an h., 2.) methylene chloride, -5 deg C to 5 deg C

2: 1.) NH₂-NH₂, KOH, 2.) aq. HCl / 1.) triethylene glycol, from 96 deg C to 215 deg C, 15 min, 2.) room temp.

With hydrogenchloride; potassium hydroxide; thionyl chloride; tin(IV) chloride; hydrazine;