N-(3-Nitropyridin-2-yl)-N-phenylacetamide

Base Information

Chemical Name:N-(3-Nitropyridin-2-yl)-N-phenylacetamide
CAS No.:88369-82-8
Molecular Formula:C13H11N3O3
Molecular Weight:257.249
Hs Code.:
DSSTox Substance ID:DTXSID20521565
Wikidata:Q82386109

Synonyms:N-(3-Nitropyridin-2-yl)-N-phenylacetamide;88369-82-8;SCHEMBL7968895;DTXSID20521565

Suppliers and Price of N-(3-Nitropyridin-2-yl)-N-phenylacetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(3-Nitropyridin-2-yl)-N-phenylacetamide

Chemical Property:

XLogP3:1.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:257.08004122
Heavy Atom Count:19
Complexity:337

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=O)N(C1=CC=CC=C1)C2=C(C=CC=N2)[N+](=O)[O-]

Technology Process of N-(3-Nitropyridin-2-yl)-N-phenylacetamide

There total 3 articles about N-(3-Nitropyridin-2-yl)-N-phenylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 34949-41-2
3-nitro-2-phenylaminopyridine

: 108-24-7
acetic anhydride

: 88369-82-8
2-N-acetyl-N-phenylamino-3-nitropyridine

Guidance literature:: With sulfuric acid; at 120 ℃; for 0.5h;

Reference yield:

: 5470-18-8,34515-82-7
2-Chloro-3-nitropyridine

: 103-84-4
Acetanilid

: 88369-82-8
2-N-acetyl-N-phenylamino-3-nitropyridine

Guidance literature:: With palladium(II) trifluoroacetate; caesium carbonate; (R)-2,2'-bis(diphenylphosphanyl)-1,1'-binaphthyl; In toluene; at 80 ℃; for 18h; Inert atmosphere;
DOI:10.1002/ejoc.201001423

Reference yield:

: 5470-18-8,34515-82-7
2-Chloro-3-nitropyridine

: 88369-82-8
2-N-acetyl-N-phenylamino-3-nitropyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / 6 h / 140 °C

2: 90 percent / conc. H₂SO₄ / 0.5 h / 120 °C

With sulfuric acid;