2,2,4-Triphenylbutanenitrile

Base Information

Chemical Name:2,2,4-Triphenylbutanenitrile
CAS No.:2961-75-3
Molecular Formula:C₂₂H₁₉N
Molecular Weight:297.4
Hs Code.:
NSC Number:82227
DSSTox Substance ID:DTXSID30292390
Wikidata:Q82030680
Mol file:2961-75-3.mol

Synonyms:2961-75-3;2,2,4-triphenylbutanenitrile;NSC82227;DTXSID30292390;NSC-82227

Suppliers and Price of 2,2,4-Triphenylbutanenitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 2,2,4-Triphenylbutanenitrile

Chemical Property:

Vapor Pressure:1.18E-07mmHg at 25°C
Boiling Point:431.6°Cat760mmHg
Flash Point:221.9°C
Density:1.088g/cm³
XLogP3:5.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:5
Exact Mass:297.151749610
Heavy Atom Count:23
Complexity:367

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)CCC(C#N)(C2=CC=CC=C2)C3=CC=CC=C3

Technology Process of 2,2,4-Triphenylbutanenitrile

There total 2 articles about 2,2,4-Triphenylbutanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 86-29-3
Diphenylacetonitrile

: 103-63-9
1-phenyl-2-bromoethane

: 2961-75-3
α-<2-Phenyl-aethyl>-diphenylacetonitril

Guidance literature:: Diphenylacetonitrile; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 0.5h; Schlenk technique;

1-phenyl-2-bromoethane; In tetrahydrofuran; at 20 ℃; for 12h; Schlenk technique;
DOI:10.1002/anie.201501122

Reference yield:

: 2961-75-3
α-<2-Phenyl-aethyl>-diphenylacetonitril

Guidance literature:: Zutropfen von Naphthalin-natrium -lsg., 1) zu Diphenylacetonitril , 2) Zugabe von 2-Phenyl-aethylbromid-Lsg. in THF bei 20grad;

Reference yield:

: 2961-75-3
α-<2-Phenyl-aethyl>-diphenylacetonitril

: 1-tosyl-2,4,4-triphenylpyrrolidine

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / diethyl ether / 2 h / Schlenk technique; Reflux

2: pyridine / 0 - 20 °C

3: benzol; iodine / 1,2-dichloro-ethane / 12 h / 25 °C / Schlenk technique; Inert atmosphere; Irradiation

With pyridine; lithium aluminium tetrahydride; benzol; iodine; In diethyl ether; 1,2-dichloro-ethane; 3: |Hofmann-Loeffler-Freytag Synthesis;
DOI:10.1002/anie.201501122