Technology Process of 1-Pyrrolidinecarboxylic acid, 3-(3-aminophenyl)-, methyl ester
There total 3 articles about 1-Pyrrolidinecarboxylic acid, 3-(3-aminophenyl)-, methyl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen;
Wilkinson's catalyst;
In
methanol;
at 20 ℃;
under 2068.65 Torr;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: silver (II) carbonate; N-ethyl-N,N-diisopropylamine / palladium diacetate; tris-(o-tolyl)phosphine / N,N-dimethyl-formamide / 9 h / 100 °C
2: hydrogen / Wilkinson's catalyst / methanol / 20 °C / 2068.65 Torr
With
silver (II) carbonate; hydrogen; N-ethyl-N,N-diisopropylamine;
palladium diacetate; Wilkinson's catalyst; tris-(o-tolyl)phosphine;
In
methanol; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: Grubbs catalyst first generation / dichloromethane / 62.17 h / 20 °C
2: silver (II) carbonate; N-ethyl-N,N-diisopropylamine / palladium diacetate; tris-(o-tolyl)phosphine / N,N-dimethyl-formamide / 9 h / 100 °C
3: hydrogen / Wilkinson's catalyst / methanol / 20 °C / 2068.65 Torr
With
silver (II) carbonate; hydrogen; N-ethyl-N,N-diisopropylamine;
palladium diacetate; Wilkinson's catalyst; Grubbs catalyst first generation; tris-(o-tolyl)phosphine;
In
methanol; dichloromethane; N,N-dimethyl-formamide;