(2-Hydroxy-3-methoxyphenyl)(2,4,6-trimethoxyphenyl)methanone

Base Information

Chemical Name:(2-Hydroxy-3-methoxyphenyl)(2,4,6-trimethoxyphenyl)methanone
CAS No.:6343-00-6
Molecular Formula:C17H18O6
Molecular Weight:318.326
Hs Code.:
NSC Number:46684
DSSTox Substance ID:DTXSID60286626
Nikkaji Number:J549.816C
Wikidata:Q82022399

Synonyms:6343-00-6;(2-hydroxy-3-methoxyphenyl)(2,4,6-trimethoxyphenyl)methanone;NSC46684;SCHEMBL8480824;DTXSID60286626;NSC-46684

Suppliers and Price of (2-Hydroxy-3-methoxyphenyl)(2,4,6-trimethoxyphenyl)methanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of (2-Hydroxy-3-methoxyphenyl)(2,4,6-trimethoxyphenyl)methanone

Chemical Property:

Vapor Pressure:8.62E-12mmHg at 25°C
Boiling Point:528.6°Cat760mmHg
Flash Point:193.6°C
Density:1.215g/cm³
XLogP3:3.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:6
Exact Mass:318.11033829
Heavy Atom Count:23
Complexity:373

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=CC(=C1O)C(=O)C2=C(C=C(C=C2OC)OC)OC

Technology Process of (2-Hydroxy-3-methoxyphenyl)(2,4,6-trimethoxyphenyl)methanone

There total 2 articles about (2-Hydroxy-3-methoxyphenyl)(2,4,6-trimethoxyphenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 621-23-8
1,2,3-trimethoxybenzene

: 7169-06-4
2,3-dimethoxybenzoyl chloride

: 6343-00-6
2-hydroxy-2',3,4',6'-tetramethoxybenzophenone

Guidance literature:: With aluminium trichloride; In dichloromethane; at 20 ℃; for 15h;
DOI:10.1016/j.tet.2004.01.033

Reference yield:

: 1521-38-6
2,3-dimethoxybenzoic acid

: 6343-00-6
2-hydroxy-2',3,4',6'-tetramethoxybenzophenone

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl chloride / CH₂Cl₂ / 3 h / 20 °C

2: 86 percent / AlCl₃ / CH₂Cl₂ / 15 h / 20 °C

With aluminium trichloride; oxalyl dichloride; In dichloromethane;
DOI:10.1016/j.tet.2004.01.033

Reference yield:

: 6343-00-6
2-hydroxy-2',3,4',6'-tetramethoxybenzophenone

: 33390-41-9
8-deoxygartanin

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / pyridine; aq. tetramethylammonium hydroxide / 4 h / Heating

2: 95 percent / aq. HI; phenol / 24 h / Heating

3: 10 percent / aq. KOH / 16 h / 20 °C

With pyridine; potassium hydroxide; tetramethyl ammoniumhydroxide; hydrogen iodide; phenol;
DOI:10.1016/j.tet.2004.01.033