Benzyl (1-amino-3-methyl-1-oxobutan-2-yl)carbamate

Base Information

Chemical Name:Benzyl (1-amino-3-methyl-1-oxobutan-2-yl)carbamate
CAS No.:88463-19-8
Molecular Formula:C13H18N2O3
Molecular Weight:250.298
Hs Code.:
DSSTox Substance ID:DTXSID90560825

Synonyms:88463-19-8;N-Cbz-L-valinamide;MFCD00191170;benzyl N-(1-carbamoyl-2-methylpropyl)carbamate;Benzyl (1-amino-3-methyl-1-oxobutan-2-yl)carbamate;SCHEMBL7331078;DTXSID90560825;SY042612;EN300-7079602

Suppliers and Price of Benzyl (1-amino-3-methyl-1-oxobutan-2-yl)carbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzyl (1-amino-3-methyl-1-oxobutan-2-yl)carbamate

Chemical Property:

XLogP3:1.7
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:6
Exact Mass:250.13174244
Heavy Atom Count:18
Complexity:286

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)C(C(=O)N)NC(=O)OCC1=CC=CC=C1

Technology Process of Benzyl (1-amino-3-methyl-1-oxobutan-2-yl)carbamate

There total 4 articles about Benzyl (1-amino-3-methyl-1-oxobutan-2-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1149-26-4,1685-33-2,92077-76-4,3588-63-4
N-benzyloxycarbonylvaline

: 88463-19-8
Benzyloxycarbonylvalinamid

Guidance literature:: With ammonium hydroxide; chloroformic acid ethyl ester; triethylamine; In tetrahydrofuran; at 0 ℃; for 0.5h;
DOI:10.1021/ol0708020

Reference yield:

: 516-06-3,25609-85-2,7004-03-7,921-10-8
D,L-valine

: 88463-19-8
Benzyloxycarbonylvalinamid

Guidance literature:: Multi-step reaction with 2 steps

1: NaHCO₃ / H₂O

2: ethyl chloroformate; aq. ammonia; triethylamine / tetrahydrofuran / 0.5 h / 0 °C

With ammonium hydroxide; chloroformic acid ethyl ester; sodium hydrogencarbonate; triethylamine; In tetrahydrofuran; water;
DOI:10.1021/ol0708020

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 88463-19-8
Benzyloxycarbonylvalinamid

Guidance literature:: Multi-step reaction with 2 steps

1: NaHCO₃ / H₂O

2: ethyl chloroformate; aq. ammonia; triethylamine / tetrahydrofuran / 0.5 h / 0 °C

With ammonium hydroxide; chloroformic acid ethyl ester; sodium hydrogencarbonate; triethylamine; In tetrahydrofuran; water;
DOI:10.1021/ol0708020