2-(2-Methoxy-5-methylphenyl)pyrazolo[1,5-a]pyridine

Base Information

Chemical Name:2-(2-Methoxy-5-methylphenyl)pyrazolo[1,5-a]pyridine
CAS No.:88467-87-2
Molecular Formula:C15H14N2O
Molecular Weight:238.289
Hs Code.:
DSSTox Substance ID:DTXSID40539263
Wikidata:Q82414971

Synonyms:88467-87-2;2-(2-Methoxy-5-methylphenyl)pyrazolo[1,5-a]pyridine;SCHEMBL10920424;DTXSID40539263

Suppliers and Price of 2-(2-Methoxy-5-methylphenyl)pyrazolo[1,5-a]pyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(2-Methoxy-5-methylphenyl)pyrazolo[1,5-a]pyridine

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:238.110613074
Heavy Atom Count:18
Complexity:284

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C=C1)OC)C2=NN3C=CC=CC3=C2

Technology Process of 2-(2-Methoxy-5-methylphenyl)pyrazolo[1,5-a]pyridine

There total 4 articles about 2-(2-Methoxy-5-methylphenyl)pyrazolo[1,5-a]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 88467-86-1
2-(2-Methoxy-5-methylphenacyl)pyridin

: 88467-87-2
2-(2-Methoxy-5-methylphenyl)pyrazolo<1,5-a>pyridin

Guidance literature:: With mesitylenesulfonylhydroxylamine; In dichloromethane; for 15h; Ambient temperature;
DOI:10.1002/hlca.19850680107

Reference yield:

: 109-06-8
α-picoline

: 88467-87-2
2-(2-Methoxy-5-methylphenyl)pyrazolo<1,5-a>pyridin

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / 1.) BuLi / hexane; diethyl ether / 0.5 h / Heating

2: 62 percent / O-(Mesitylsulfonyl)hydroxylamin / CH₂Cl₂ / 15 h / Ambient temperature

With n-butyllithium; mesitylenesulfonylhydroxylamine; In diethyl ether; hexane; dichloromethane;
DOI:10.1002/hlca.19850680107

Reference yield:

: 63113-79-1
methyl 2-methoxy-5-methylbenzoate

: 88467-87-2
2-(2-Methoxy-5-methylphenyl)pyrazolo<1,5-a>pyridin

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / 1.) BuLi / hexane; diethyl ether / 0.5 h / Heating

2: 62 percent / O-(Mesitylsulfonyl)hydroxylamin / CH₂Cl₂ / 15 h / Ambient temperature

With n-butyllithium; mesitylenesulfonylhydroxylamine; In diethyl ether; hexane; dichloromethane;
DOI:10.1002/hlca.19850680107