4-Penten-1-ol, 2-[(phenylmethoxy)methyl]-, (R)-

Base Information

Chemical Name:4-Penten-1-ol, 2-[(phenylmethoxy)methyl]-, (R)-
CAS No.:88481-68-9
Molecular Formula:C13H18O2
Molecular Weight:206.285
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Penten-1-ol, 2-[(phenylmethoxy)methyl]-, (R)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-Penten-1-ol, 2-[(phenylmethoxy)methyl]-, (R)-

There total 23 articles about 4-Penten-1-ol, 2-[(phenylmethoxy)methyl]-, (R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₃H₁₆O₂

: 88481-68-9
(R)-2-((benzyloxy)methyl)pent-4-en-1-ol

Guidance literature:: With sodium tetrahydroborate; water; In methanol; at 20 ℃;
DOI:10.1016/j.tetlet.2011.08.006

Reference yield:

: (S)-N-benzyl-2-((benzyloxy)methyl)-N-(2-isopropylphenyl)pent-4-enamide

: 95791-03-0
(2S)-2-[(benzyloxy)methyl]pent-4-en-1-ol

: 88481-68-9
(R)-2-((benzyloxy)methyl)pent-4-en-1-ol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 25 ℃; for 2h; Overall yield = 21 mg; Schlenk technique; Sealed tube; Inert atmosphere;
DOI:10.1002/anie.202015004

Reference yield:

: 42201-43-4
2-allyl-1,3-propanediol

: 88481-68-9
(R)-2-((benzyloxy)methyl)pent-4-en-1-ol

Guidance literature:: Multi-step reaction with 5 steps

1: tetrahydrofuran / 24 h / pig pancreatic lipase (PPL)

2: N,N-diisopropylethylamine / CH₂Cl₂ / 2 h

3: 1 M aq. NaOH / 24 h

4: 1.) NaH / 1.) DMF, RT, 1 h, 2.) DMF, overnight

5: MeOH, TsOH / 48 h / Heating

With methanol; sodium hydroxide; sodium hydride; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1246/bcsj.69.735