6-(6-pentylundecyl)-1,2,3,4-tetrahydronaphthalene

Base Information

• Chemical Name: 6-(6-pentylundecyl)-1,2,3,4-tetrahydronaphthalene
• CAS No.: 2656-02-2
• Molecular Formula: C26H44
• Molecular Weight: 356.6276
• Mol file: 2656-02-2.mol

Synonyms:

Chemical Property of 6-(6-pentylundecyl)-1,2,3,4-tetrahydronaphthalene

Chemical Property:

• Vapor Pressure: 3.69E-08mmHg at 25°C
• Boiling Point: 458.6°Cat760mmHg
• Flash Point: 220.6°C
• Density: 0.89g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 6-(6-pentylundecyl)-1,2,3,4-tetrahydronaphthalene

There total 6 articles about 6-(6-pentylundecyl)-1,2,3,4-tetrahydronaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(5,6,7,8-tetrahydro-[2]naphthyl)-butan-1-ol (2928-93-0) → 1--6-pentyl-undecan (2656-02-2)

Guidance literature:

Multi-step reaction with 5 steps

1: aq. HBr

2: ethanol / Heating

3: (i) aq. KOH, (ii) (heating)

4: H₂SO₄

5: (i) Et₂O, (ii) oxalic acid, (iii) H₂, Pd-BaSO₄, AcOH

With sulfuric acid; hydrogen bromide; In ethanol;

Reference yield:

6-(4-bromo-butyl)-1,2,3,4-tetrahydro-naphthalene (2655-98-3) → 1--6-pentyl-undecan (2656-02-2)

Guidance literature:

Multi-step reaction with 4 steps

1: ethanol / Heating

2: (i) aq. KOH, (ii) (heating)

3: H₂SO₄

4: (i) Et₂O, (ii) oxalic acid, (iii) H₂, Pd-BaSO₄, AcOH

With sulfuric acid; In ethanol;

Reference yield:

methyl 4-(5,6,7,8-tetrahydronaphthalen-2-yl)butanoate (785-18-2) → 1--6-pentyl-undecan (2656-02-2)

Guidance literature:

Multi-step reaction with 6 steps

1: LiAlH₄ / diethyl ether

2: aq. HBr

3: ethanol / Heating

4: (i) aq. KOH, (ii) (heating)

5: H₂SO₄

6: (i) Et₂O, (ii) oxalic acid, (iii) H₂, Pd-BaSO₄, AcOH

With lithium aluminium tetrahydride; sulfuric acid; hydrogen bromide; In diethyl ether; ethanol;

upstream raw materials:

6-(Tetralyl-6)-capronsaeure-methylester

n-pentylmagnesium bromide

4-(5,6,7,8-tetrahydro-[2]naphthyl)-butan-1-ol

6-(4-bromo-butyl)-1,2,3,4-tetrahydro-naphthalene