pentacyclo[7.3.1.1~4,12~.0~2,7~.0~6,11~]tetradecan-4-ol (non-preferred name)

Base Information

• Chemical Name: pentacyclo[7.3.1.1~4,12~.0~2,7~.0~6,11~]tetradecan-4-ol (non-preferred name)
• CAS No.: 30651-03-7
• Molecular Formula: C14H20 O
• Molecular Weight: 204.312
• Mol file: 30651-03-7.mol

Synonyms:4-Diamantanol;4-Hydroxydiamantane

Chemical Property of pentacyclo[7.3.1.1~4,12~.0~2,7~.0~6,11~]tetradecan-4-ol (non-preferred name)

Chemical Property:

• Vapor Pressure: 1.51E-05mmHg at 25°C
• Boiling Point: 327.6°Cat760mmHg
• Flash Point: 137.9°C
• Density: 1.244g/cm³

Purity/Quality:

99% ^*data from raw suppliers

4-Hydroxydiamantane 95 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of pentacyclo[7.3.1.1~4,12~.0~2,7~.0~6,11~]tetradecan-4-ol (non-preferred name)

There total 19 articles about pentacyclo[7.3.1.1~4,12~.0~2,7~.0~6,11~]tetradecan-4-ol (non-preferred name) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

4-(tert-butyldimethylsiloxy)diamantane → 4-hydroxydiamantane (30651-03-7)

Guidance literature:

With hydrogenchloride; water; In methanol; chloroform; at 20 ℃; for 7h;

DOI:10.1055/s-0033-1338583

Reference yield: 85.0%

4-bromo-diamantane (30545-30-3) → 4-hydroxydiamantane (30651-03-7)

Guidance literature:

With nitric acid; at 50 ℃;

Reference yield: 82.0%

diamantane → 4-hydroxydiamantane (30651-03-7) + 1-hydroxydiamantane

Guidance literature:

diamantane; With nitric acid; In dichloromethane; at 0 - 20 ℃; for 1h;

With water; for 1.5h; Heating;

DOI:10.1002/chem.200500031

upstream raw materials:

diamantane

diamantan-1-ol

3-hydroxydiamantane

4-bromo-diamantane

Downstream raw materials:

diamantane

4-diamantylacetic acid

3,9-diamantanebisacetic acid

4,9-diamantanebisacetic acid

Refernces

• 1、 Khusnutdinov,Shchadneva,Mukhametshina,Dzhemilev. "Selective hydroxylation of adamantane and its derivatives". scheme or table. p. 1137 - 1142. Retrieved 2009/12/03.
• 2、 -. "Diamondoid derivatives possessing therapeutic activity in the treatment of neurologic disorders". Page/Page column 20-23. . Retrieved 2008/06/13.