1H-Indene-1,2(3H)-dione, 5-(phenylmethoxy)-, 2-oxime

Base Information

Chemical Name:1H-Indene-1,2(3H)-dione, 5-(phenylmethoxy)-, 2-oxime
CAS No.:88628-63-1
Molecular Formula:C16H13NO3
Molecular Weight:267.284
Hs Code.:

Synonyms:

Suppliers and Price of 1H-Indene-1,2(3H)-dione, 5-(phenylmethoxy)-, 2-oxime

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1H-Indene-1,2(3H)-dione, 5-(phenylmethoxy)-, 2-oxime

Chemical Property:

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1H-Indene-1,2(3H)-dione, 5-(phenylmethoxy)-, 2-oxime

There total 4 articles about 1H-Indene-1,2(3H)-dione, 5-(phenylmethoxy)-, 2-oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 78326-88-2
5-benzyloxy-1-indanone

: 88628-63-1
5-Benzyloxy-indan-1,2-dione 2-oxime

Guidance literature:: With hydrogenchloride; isopentyl nitrite; In methanol; at 50 ℃; for 0.5h;
DOI:10.1248/cpb.31.2329

Reference yield:

: 3470-49-3
5-hydroxy-2,3-dihydro-1H-indene-1-one

: 88628-63-1
5-Benzyloxy-indan-1,2-dione 2-oxime

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / K₂CO₃/KI / dimethylformamide / 2 h / 100 °C

2: 70 percent / isoamilnitrite/conc. HCl / methanol / 0.5 h / 50 °C

With hydrogenchloride; potassium carbonate; potassium iodide; isopentyl nitrite; In methanol; N,N-dimethyl-formamide;
DOI:10.1248/cpb.31.2329

Reference yield:

: 5111-70-6
5-methoxy-1-indanone

: 88628-63-1
5-Benzyloxy-indan-1,2-dione 2-oxime

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / AlCl₃ / benzene / 1 h / Heating

2: 79 percent / K₂CO₃/KI / dimethylformamide / 2 h / 100 °C

3: 70 percent / isoamilnitrite/conc. HCl / methanol / 0.5 h / 50 °C

With hydrogenchloride; aluminium trichloride; potassium carbonate; potassium iodide; isopentyl nitrite; In methanol; N,N-dimethyl-formamide; benzene;
DOI:10.1248/cpb.31.2329