(Z)-2-Hydroxy-6-(tridec-8-en-1-yl)benzoic acid

Base Information

Chemical Name:(Z)-2-Hydroxy-6-(tridec-8-en-1-yl)benzoic acid
CAS No.:88640-88-4
Molecular Formula:C₂₀H₃₀O₃
Molecular Weight:318.456
Hs Code.:
ChEMBL ID:CHEMBL4589399
DSSTox Substance ID:DTXSID501243022
Nikkaji Number:J694.966E

Synonyms:88640-88-4;CHEMBL4589399;DTXSID501243022;(Z)-2-Hydroxy-6-(tridec-8-en-1-yl)benzoic acid;Benzoic acid, 2-hydroxy-6-(8-tridecenyl)-, (Z)-

Suppliers and Price of (Z)-2-Hydroxy-6-(tridec-8-en-1-yl)benzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of (Z)-2-Hydroxy-6-(tridec-8-en-1-yl)benzoic acid

Chemical Property:

XLogP3:7.5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:12
Exact Mass:318.21949481
Heavy Atom Count:23
Complexity:338

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCC=CCCCCCCCC1=C(C(=CC=C1)O)C(=O)O
Isomeric SMILES:CCCC/C=C\CCCCCCCC1=C(C(=CC=C1)O)C(=O)O

Technology Process of (Z)-2-Hydroxy-6-(tridec-8-en-1-yl)benzoic acid

There total 9 articles about (Z)-2-Hydroxy-6-(tridec-8-en-1-yl)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10160-26-6
9-(2-tetrahydropyranyloxy)-1-nonyne

: 88640-88-4
2-Hydroxy-6-<(Z)-8-tridecenyl>benzoic acid

Guidance literature:: Multi-step reaction with 9 steps

1: n-BuLi / tetrahydrofuran; hexane / 1.) 0 deg C, 30 min, 2.) r.t., 70 min

2: p-TsOH*H₂O / methanol / 1 h / Ambient temperature

3: 99 percent / pyridine / 3.5 h / Ambient temperature

4: 73 percent / dichloromaleic anhydride / 200 °C

5: 99 percent / 2 M KOH / ethanol / 19 h / Heating

6: 72 percent / CBr₄, PPh₃ / CH₂Cl₂ / 6 h / Ambient temperature

7: 66 percent / n-BuLi / tetrahydrofuran; hexane; hexamethylphosphoric acid triamide / 1.) -60 deg C, 30 min, 2.) r.t., 16 h

8: 99 percent / H₂, quinoline / 5percent Pd/CaCO₃ / cyclohexane / 0.32 h / 750.06 Torr

9: 66 percent / AlI₃, cyclohexene / CS₂ / Heating

With pyridine; quinoline; potassium hydroxide; aluminium(III) iodide; n-butyllithium; dichloromaleic acid anhydride; carbon tetrabromide; hydrogen; toluene-4-sulfonic acid; triphenylphosphine; cyclohexene; Lindlar's catalyst; In tetrahydrofuran; methanol; carbon disulfide; N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; hexane; dichloromethane; cyclohexane;

Reference yield:

: 10160-28-8
8-nonyn-1-ol

: 88640-88-4
2-Hydroxy-6-<(Z)-8-tridecenyl>benzoic acid

Guidance literature:: Multi-step reaction with 10 steps

1: p-TsOH*H₂O / 2 h / Ambient temperature

2: n-BuLi / tetrahydrofuran; hexane / 1.) 0 deg C, 30 min, 2.) r.t., 70 min

3: p-TsOH*H₂O / methanol / 1 h / Ambient temperature

4: 99 percent / pyridine / 3.5 h / Ambient temperature

5: 73 percent / dichloromaleic anhydride / 200 °C

6: 99 percent / 2 M KOH / ethanol / 19 h / Heating

7: 72 percent / CBr₄, PPh₃ / CH₂Cl₂ / 6 h / Ambient temperature

8: 66 percent / n-BuLi / tetrahydrofuran; hexane; hexamethylphosphoric acid triamide / 1.) -60 deg C, 30 min, 2.) r.t., 16 h

9: 99 percent / H₂, quinoline / 5percent Pd/CaCO₃ / cyclohexane / 0.32 h / 750.06 Torr

10: 66 percent / AlI₃, cyclohexene / CS₂ / Heating

With pyridine; quinoline; potassium hydroxide; aluminium(III) iodide; n-butyllithium; dichloromaleic acid anhydride; carbon tetrabromide; hydrogen; toluene-4-sulfonic acid; triphenylphosphine; cyclohexene; Lindlar's catalyst; In tetrahydrofuran; methanol; carbon disulfide; N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; hexane; dichloromethane; cyclohexane;

Reference yield:

: 131271-31-3
methyl 10-<(tetrahydropyran-2'-yl)oxy>-2-decynoate

: 88640-88-4
2-Hydroxy-6-<(Z)-8-tridecenyl>benzoic acid

Guidance literature:: Multi-step reaction with 8 steps

1: p-TsOH*H₂O / methanol / 1 h / Ambient temperature

2: 99 percent / pyridine / 3.5 h / Ambient temperature

3: 73 percent / dichloromaleic anhydride / 200 °C

4: 99 percent / 2 M KOH / ethanol / 19 h / Heating

5: 72 percent / CBr₄, PPh₃ / CH₂Cl₂ / 6 h / Ambient temperature

6: 66 percent / n-BuLi / tetrahydrofuran; hexane; hexamethylphosphoric acid triamide / 1.) -60 deg C, 30 min, 2.) r.t., 16 h

7: 99 percent / H₂, quinoline / 5percent Pd/CaCO₃ / cyclohexane / 0.32 h / 750.06 Torr

8: 66 percent / AlI₃, cyclohexene / CS₂ / Heating

With pyridine; quinoline; potassium hydroxide; aluminium(III) iodide; n-butyllithium; dichloromaleic acid anhydride; carbon tetrabromide; hydrogen; toluene-4-sulfonic acid; triphenylphosphine; cyclohexene; Lindlar's catalyst; In tetrahydrofuran; methanol; carbon disulfide; N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; hexane; dichloromethane; cyclohexane;