1,4-Cycloheptadiene, (Z,Z)-

Base Information

• Chemical Name: 1,4-Cycloheptadiene, (Z,Z)-
• CAS No.: 88728-00-1
• Molecular Formula: C₇H₁₀
• Molecular Weight: 94.1564

Synonyms:

Chemical Property of 1,4-Cycloheptadiene, (Z,Z)-

Chemical Property:

Purity/Quality:

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Technology Process of 1,4-Cycloheptadiene, (Z,Z)-

There total 6 articles about 1,4-Cycloheptadiene, (Z,Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

Cyclohepta-1,3,5-triene (544-25-2) → Cyclohepta-1,3-diene (876938-53-3) + 1,3-cycloheptadiene (7161-35-5,88728-00-1,88728-01-2,88728-02-3) + Cycloheptene (628-92-2,45509-99-7) + toluene (108-88-3,15644-74-3,16713-13-6)

Guidance literature:

With 9,10-dihydroanthracene; In diphenylether; at 279 ℃; Rate constant; Thermodynamic data; various temp., solvents; ΔG(excit.), ΔH(excit.), ΔS(excit.), ΔH_R, deuterium isotope effects;

DOI:10.1002/jlac.199619961006

Reference yield:

Cyclohepta-1,3,5-triene (544-25-2) → Cyclohepta-1,3-diene (876938-53-3) + 1,3-cycloheptadiene (7161-35-5,88728-00-1,88728-01-2,88728-02-3) + Cycloheptene (628-92-2,45509-99-7)

Guidance literature:

With hydrogen; potassium cyanide; potassium hydroxide; potassium chloride; β‐cyclodextrin; cobalt(II) chloride; In benzene; for 36h; under 760 Torr; Yield given. Yields of byproduct given; Ambient temperature;

DOI:10.1021/jo00293a034

Reference yield:

Cyclohepta-1,3,5-triene (544-25-2) → 1,3-cycloheptadiene (7161-35-5,88728-00-1,88728-01-2,88728-02-3) + Cycloheptene (628-92-2,45509-99-7)

Guidance literature:

With Amberlite IRA-400; borohydride form; copper(II) sulfate; In methanol; at 20 ℃; for 6h;

DOI:10.1246/bcsj.70.1101

upstream raw materials:

furan

(1S,2S,4R,5R)-6,7-Diaza-tricyclo[3.2.2.0^2,4]non-6-ene

3-norcarene

Cyclohepta-1,3,5-triene

Downstream raw materials:

Bicyclo<5.1.0>octen-(3)

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