4-Amino-1-methyl-3-nitroquinolin-2(1H)-one

Base Information

Chemical Name:4-Amino-1-methyl-3-nitroquinolin-2(1H)-one
CAS No.:141945-48-4
Molecular Formula:C₁₀H₉N₃O₃
Molecular Weight:219.2
Hs Code.:
DSSTox Substance ID:DTXSID00383027
Wikidata:Q82174574
Mol file:141945-48-4.mol

Synonyms:4-Amino-1-methyl-3-nitroquinolin-2(1H)-one;Cambridge id 5807837;Oprea1_068994;DTXSID00383027;AKOS000633474;141945-48-4;CS-0300843;Z56782706

Suppliers and Price of 4-Amino-1-methyl-3-nitroquinolin-2(1H)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 4-Amino-1-methyl-3-nitroquinolin-2(1H)-one

Chemical Property:

Vapor Pressure:0.000519mmHg at 25°C
Boiling Point:312.7°Cat760mmHg
Flash Point:142.9°C
PSA：93.84000
Density:1.46g/cm³
LogP:2.13330
XLogP3:1.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:0
Exact Mass:219.06439116
Heavy Atom Count:16
Complexity:372

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1C2=CC=CC=C2C(=C(C1=O)[N+](=O)[O-])N

Technology Process of 4-Amino-1-methyl-3-nitroquinolin-2(1H)-one

There total 5 articles about 4-Amino-1-methyl-3-nitroquinolin-2(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 79966-13-5
4-chloro-1-methyl-3-nitro-2-(1H)quinolinone

: 141945-48-4
4-amino-1-methyl-3-nitro-2(1H)-quinolone

Guidance literature:: With ammonia; In various solvent(s); for 0.5h;

Reference yield: 91.0%

: 141945-45-1
1-methyl-3-nitro-4-triphenylphosphoranylidene-amino-2(1H)-quinolone

: 141945-48-4
4-amino-1-methyl-3-nitro-2(1H)-quinolone

Guidance literature:: With acetic acid; for 1h; Heating;

Reference yield:

: 1677-46-9
4-hydroxy-1-methyl-2(1H)-quinolone

: 141945-48-4
4-amino-1-methyl-3-nitro-2(1H)-quinolone

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / conc. HNO₃, NaNO₂ / acetic acid / 0.5 h

2: 92 percent / triethylamine, phosphoryl chloride / 1 h / Heating

3: 91 percent / NH₃ (gas) / various solvent(s) / 0.5 h

With ammonia; nitric acid; triethylamine; sodium nitrite; trichlorophosphate; In acetic acid;