6-[(E)-(carbamothioylhydrazinylidene)methyl]pyridine-2-carbothioamide

Base Information

Chemical Name:6-[(E)-(carbamothioylhydrazinylidene)methyl]pyridine-2-carbothioamide
CAS No.:78797-11-2
Molecular Formula:C₈H₉N₅S₂
Molecular Weight:239.325
Hs Code.:
NSC Number:320596
DSSTox Substance ID:DTXSID20429916

Synonyms:NSC320596;78797-11-2;DTXSID20429916;NSC-320596

Suppliers and Price of 6-[(E)-(carbamothioylhydrazinylidene)methyl]pyridine-2-carbothioamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 6-[(E)-(carbamothioylhydrazinylidene)methyl]pyridine-2-carbothioamide

Chemical Property:

Vapor Pressure:2.26E-09mmHg at 25°C
Boiling Point:480°Cat760mmHg
Flash Point:244.1°C
Density:1.51g/cm³
XLogP3:0.3
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:239.02993766
Heavy Atom Count:15
Complexity:278

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC(=NC(=C1)C(=S)N)C=NNC(=S)N
Isomeric SMILES:C1=CC(=NC(=C1)C(=S)N)/C=N/NC(=S)N

Technology Process of 6-[(E)-(carbamothioylhydrazinylidene)methyl]pyridine-2-carbothioamide

There total 2 articles about 6-[(E)-(carbamothioylhydrazinylidene)methyl]pyridine-2-carbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 79-19-6
thiosemicarbazide

: 78797-07-6
6-(diacetoxymethyl)pyridine-2-carbothioamide

: 78797-11-2
6-formylpyridine-2-carbothioamide thiosemicarbazone

Guidance literature:: With hydrogenchloride; In ethanol; for 5h; Heating;
DOI:10.1021/jm00142a012

Reference yield:

: 78797-06-5
2-cyano-6-(diacetoxymethyl)pyridine

: 78797-11-2
6-formylpyridine-2-carbothioamide thiosemicarbazone

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / (C₂H₅)3N, pyridine, H₂S / 1 h

2: 70 percent / concd. HCl / ethanol / 5 h / Heating

With pyridine; hydrogenchloride; hydrogen sulfide; triethylamine; In ethanol;
DOI:10.1021/jm00142a012