1,5-Diazocin-2(1H)-one, 1-(4-chlorobutyl)hexahydro-5-methyl-4-phenyl-

Base Information

Chemical Name:1,5-Diazocin-2(1H)-one, 1-(4-chlorobutyl)hexahydro-5-methyl-4-phenyl-
CAS No.:88909-11-9
Molecular Formula:C₁₇H₂₅ClN₂O
Molecular Weight:308.851
Hs Code.:

Synonyms:

Suppliers and Price of 1,5-Diazocin-2(1H)-one, 1-(4-chlorobutyl)hexahydro-5-methyl-4-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of 1,5-Diazocin-2(1H)-one, 1-(4-chlorobutyl)hexahydro-5-methyl-4-phenyl-

Chemical Property:

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,5-Diazocin-2(1H)-one, 1-(4-chlorobutyl)hexahydro-5-methyl-4-phenyl-

There total 8 articles about 1,5-Diazocin-2(1H)-one, 1-(4-chlorobutyl)hexahydro-5-methyl-4-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 31925-54-9
(R,S)-N-(2-cyanoethyl)-N-methyl-β-phenyl-β-alanine

: 88909-11-9
(R,S)-1-(4-chlorobutyl)-5-methyl-4-phenyl-1,5-diazacyclooctan-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: 59 percent / H₂, 2 M aq. HCl / PtO₂ / ethanol / 18 h / 760 Torr / Ambient temperature

2: 94 percent / 2,2'-dithiodipyridine, PPh₃ / acetonitrile / 12 h / Heating

3: 57 percent / KOH, DMSO / 6 h

With hydrogenchloride; potassium hydroxide; 2,2'-dipyridyldisulphide; hydrogen; dimethyl sulfoxide; triphenylphosphine; platinum(IV) oxide; In ethanol; acetonitrile;

Reference yield:

: 76497-43-3
(R,S)-N-methyl-β-phenyl-β-alanine

: 88909-11-9
(R,S)-1-(4-chlorobutyl)-5-methyl-4-phenyl-1,5-diazacyclooctan-2-one

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / 50percent aq. KOH

2: 59 percent / H₂, 2 M aq. HCl / PtO₂ / ethanol / 18 h / 760 Torr / Ambient temperature

3: 94 percent / 2,2'-dithiodipyridine, PPh₃ / acetonitrile / 12 h / Heating

4: 57 percent / KOH, DMSO / 6 h

With hydrogenchloride; potassium hydroxide; 2,2'-dipyridyldisulphide; hydrogen; dimethyl sulfoxide; triphenylphosphine; platinum(IV) oxide; In ethanol; acetonitrile;

Reference yield:

: 88931-10-6
(R,S)-N-(2-aminopropyl)-N-methyl-β-phenyl-β-alanine

: 88909-11-9
(R,S)-1-(4-chlorobutyl)-5-methyl-4-phenyl-1,5-diazacyclooctan-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / di-2-pyridyl disulphide, Ph₃P / acetonitrile / Heating

2: KOH / dimethylsulfoxide

With potassium hydroxide; 2,2'-dipyridyldisulphide; triphenylphosphine; In dimethyl sulfoxide; acetonitrile;
DOI:10.1039/c39830000960