1,2,5-Trioxaspiro[5.5]undecan-9-one, 3-[1-(4-chlorophenyl)ethenyl]-

Base Information

Chemical Name:1,2,5-Trioxaspiro[5.5]undecan-9-one, 3-[1-(4-chlorophenyl)ethenyl]-
CAS No.:889099-43-8
Molecular Formula:C16H17ClO4
Molecular Weight:308.762
Hs Code.:
ChEMBL ID:CHEMBL206948
DSSTox Substance ID:DTXSID10469048

Synonyms:889099-43-8;1,2,5-Trioxaspiro[5.5]undecan-9-one, 3-[1-(4-chlorophenyl)ethenyl]-;CHEMBL206948;SCHEMBL4487338;DTXSID10469048

Suppliers and Price of 1,2,5-Trioxaspiro[5.5]undecan-9-one, 3-[1-(4-chlorophenyl)ethenyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1,2,5-Trioxaspiro[5.5]undecan-9-one, 3-[1-(4-chlorophenyl)ethenyl]-

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:308.0815367
Heavy Atom Count:21
Complexity:405

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=C(C1COC2(CCC(=O)CC2)OO1)C3=CC=C(C=C3)Cl

Technology Process of 1,2,5-Trioxaspiro[5.5]undecan-9-one, 3-[1-(4-chlorophenyl)ethenyl]-

There total 1 articles about 1,2,5-Trioxaspiro[5.5]undecan-9-one, 3-[1-(4-chlorophenyl)ethenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 93404-36-5,148183-95-3,132533-09-6
(2E)-3-(4'-chlorophenyl)but-2-en-1-ol

: 889099-43-8
3-[1-(4-Chloro-phenyl)-vinyl]-1,2,5-trioxa-spiro[5.5]undecan-9-one

Guidance literature:: Multi-step reaction with 2 steps

1: O₂; methylene blue / acetonitrile / 4 h / -10 - 0 °C / Irradiation

2: aq. HCl / acetonitrile / 18 h / 5 °C

With hydrogenchloride; oxygen; methylene blue; In acetonitrile;
DOI:10.1021/jm051130r

Reference yield: 93.0%

: 889099-43-8
3-[1-(4-Chloro-phenyl)-vinyl]-1,2,5-trioxa-spiro[5.5]undecan-9-one

: 889099-59-6
3-[1-(4-chloro-phenyl)-vinyl]-1,2,5-trioxa-spiro[5.5]undecan-9-ol

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 ℃; for 0.5h;
DOI:10.1021/jm051130r

Reference yield: 91.2%

: 889099-43-8
3-[1-(4-Chloro-phenyl)-vinyl]-1,2,5-trioxa-spiro[5.5]undecan-9-one

: {3-[1-(4-Chloro-phenyl)-vinyl]-1,2,5-trioxa-spiro[5.5]undec-9-ylidene}-acetic acid ethyl ester

Guidance literature:: diethoxyphosphoryl-acetic acid ethyl ester; With sodium hydride; In 1,2-dimethoxyethane; at 0 ℃; for 1h;

3-[1-(4-Chloro-phenyl)-vinyl]-1,2,5-trioxa-spiro[5.5]undecan-9-one; In 1,2-dimethoxyethane; at 0 ℃; for 0.5h;