TERT-BUTYL 4-(2-AMINOBENZOYL)PIPERAZINE-1-CARBOXYLATE

Base Information

• Chemical Name: TERT-BUTYL 4-(2-AMINOBENZOYL)PIPERAZINE-1-CARBOXYLATE
• CAS No.: 889125-00-2
• Molecular Formula: C₁₆H₂₃N₃O₃
• Molecular Weight: 305.377
• Hs Code.: 2933599090
• Mol file: 889125-00-2.mol

Synonyms:tert-butyl 4-[(2-aminophenyl)carbonyl]piperazine-1-carboxylate;tertbutylaminophenylcarbonylpiperazinecarboxylate;AB3283;4-(2-aminobenzoyl)-N-Boc-piperazine;

Chemical Property of TERT-BUTYL 4-(2-AMINOBENZOYL)PIPERAZINE-1-CARBOXYLATE

Chemical Property:

• Melting Point: 122～124℃
• PSA: 75.87000
• LogP: 2.41870

Purity/Quality:

98%min ^*data from raw suppliers

tert-Butyl 4-[(2-aminophenyl)carbonyl]piperazine-1-carboxylate >95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of TERT-BUTYL 4-(2-AMINOBENZOYL)PIPERAZINE-1-CARBOXYLATE

There total 1 articles about TERT-BUTYL 4-(2-AMINOBENZOYL)PIPERAZINE-1-CARBOXYLATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

isatoic anhydride (118-48-9) + 1-t-Butoxycarbonylpiperazine (57260-71-6) → 4-(2-aminobenzoyl) N-boc piperazine (889125-00-2)

Guidance literature:

In 1,4-dioxane; for 4h; Reflux;

DOI:10.1016/j.bmcl.2010.04.037

Reference yield:

4-(2-aminobenzoyl) N-boc piperazine (889125-00-2) + 3,4,5-trimethoxy-benzaldehyde (86-81-7) → C26H35N3O6 (1235987-65-1)

Guidance literature:

With sodium cyanoborohydride; acetic acid; In methanol; at 20 ℃; for 22h;

DOI:10.1016/j.bmcl.2010.04.037

Reference yield:

4-(2-aminobenzoyl) N-boc piperazine (889125-00-2) + 3-Formylchromone (17422-74-1) → C26H29N3O5 (1235987-68-4)

Guidance literature:

With sodium cyanoborohydride; acetic acid; In methanol; at 20 ℃; for 22h;

DOI:10.1016/j.bmcl.2010.04.037

upstream raw materials:

isatoic anhydride

1-t-Butoxycarbonylpiperazine

Downstream raw materials:

C₂₂H₂₈N₄O₃

C₂₆H₃₅N₃O₆

C₂₆H₂₉N₃O₅

C₂₇H₃₁N₃O₃

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