1-Cyanomethyl-2-(N-(1-carboxy-2-phenylethyl))iminopyrrolidine hydrate

Base Information

Chemical Name:1-Cyanomethyl-2-(N-(1-carboxy-2-phenylethyl))iminopyrrolidine hydrate
CAS No.:91417-78-6
Molecular Formula:C₁₅H₁₇N₃O₂
Molecular Weight:271.319
Hs Code.:

Synonyms:N-(1-(Cyanomethyl)-2-pyrrolidinylidene)-L-phenylalanine hydrate;1-Cyanomethyl-2-(N-(1-carboxy-2-phenylethyl))iminopyrrolidine hydrate;91417-78-6;L-Phenylalanine, N-(1-(cyanomethyl)-2-pyrrolidinylidene)-, hydrate;C15H17N3O2.H2O;C15-H17-N3-O2.H2-O;LS-105781

Suppliers and Price of 1-Cyanomethyl-2-(N-(1-carboxy-2-phenylethyl))iminopyrrolidine hydrate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Cyanomethyl-2-(N-(1-carboxy-2-phenylethyl))iminopyrrolidine hydrate

Chemical Property:

Vapor Pressure:2.03E-10mmHg at 25°C
Boiling Point:490°Cat760mmHg
Flash Point:250.2°C
Density:g/cm³
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:5
Exact Mass:289.14264148
Heavy Atom Count:21
Complexity:418

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC(=NC(CC2=CC=CC=C2)C(=O)O)N(C1)CC#N.O

Technology Process of 1-Cyanomethyl-2-(N-(1-carboxy-2-phenylethyl))iminopyrrolidine hydrate

There total 3 articles about 1-Cyanomethyl-2-(N-(1-carboxy-2-phenylethyl))iminopyrrolidine hydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 57275-83-9
nitrile of 2-oxopyrrolidine-1-acetic acid

: 91417-78-6
1-Cyanomethyl-2-iminopyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) POCl₃ / 1.) benzene, room temp., 4.5 h, 2.) EtOH, 0.5 h

2: 82 percent / ethanol / 3 h / Ambient temperature

With trichlorophosphate; In ethanol;
DOI:10.1007/BF00758995

Reference yield:

: 7491-74-9
2-oxo-1-pyrrolidine acetamide

: 91417-78-6
1-Cyanomethyl-2-iminopyrrolidine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) POCl₃, DMF, 2.) pyridine / 1.) acetonitrile, 50 deg C, 2.5 h, 2.) 0 deg C, 20 min

2: 1.) POCl₃ / 1.) benzene, room temp., 4.5 h, 2.) EtOH, 0.5 h

3: 82 percent / ethanol / 3 h / Ambient temperature

With pyridine; N,N-dimethyl-formamide; trichlorophosphate; In ethanol;
DOI:10.1007/BF00758995

Reference yield:

: 1-Cyanomethyl-2-ethoxy-1,2-dehydropyrrolidinium tetrafluoroborate

: 91417-78-6
1-Cyanomethyl-2-iminopyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / ethanol / 2 h / 5 - 10 °C

2: 82 percent / ethanol / 3 h / Ambient temperature

In ethanol;
DOI:10.1007/BF00758995