Acetic acid, [4-chloro-2-[(E)-[1-[(4-chlorophenyl)sulfonyl]hexahydro-3,7-dioxo-6H-1,4 -diazepin-6-ylidene]methyl]phenoxy]-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Acetic acid, [4-chloro-2-[(E)-[1-[(4-chlorophenyl)sulfonyl]hexahydro-3,7-dioxo-6H-1,4 -diazepin-6-ylidene]methyl]phenoxy]-, 1,1-dimethylethyl ester
CAS No.:889854-32-4
Molecular Formula:C24H24Cl2N2O7S
Molecular Weight:555.436
Hs Code.:

Acetic acid,
[4-chloro-2-[(E)-[1-[(4-chlorophenyl)sulfonyl]hexahydro-3,7-dioxo-6H-1,4
-diazepin-6-ylidene]methyl]phenoxy]-, 1,1-dimethylethyl ester

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Chemical Property of Acetic acid, [4-chloro-2-[(E)-[1-[(4-chlorophenyl)sulfonyl]hexahydro-3,7-dioxo-6H-1,4 -diazepin-6-ylidene]methyl]phenoxy]-, 1,1-dimethylethyl ester

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Technology Process of Acetic acid, [4-chloro-2-[(E)-[1-[(4-chlorophenyl)sulfonyl]hexahydro-3,7-dioxo-6H-1,4 -diazepin-6-ylidene]methyl]phenoxy]-, 1,1-dimethylethyl ester

There total 7 articles about Acetic acid, [4-chloro-2-[(E)-[1-[(4-chlorophenyl)sulfonyl]hexahydro-3,7-dioxo-6H-1,4 -diazepin-6-ylidene]methyl]phenoxy]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 889858-30-4
(6E)-6-(5-chloro-2-hydroxybenzylidene)-4-[(4-chlorophenyl)sulfonyl]-1,4-diazepan-2,5-dione

: 5292-43-3
bromoacetic acid tert-butyl ester

: 889854-32-4
tert-butyl [4-chloro-2-((E)-{1-[(4-chlorophenyl)sulfonyl]-3,7-dioxo-1,4-diazepan-6-ylidene}methyl)phenoxy]acetate

Guidance literature:: With sodium hydrogencarbonate; sodium iodide; In N,N-dimethyl-formamide; at 20 ℃; for 20h;
DOI:10.1016/j.bmcl.2007.03.038

Reference yield:

: 945013-29-6
C₁₇H₂₁ClO₆

: 889854-32-4
tert-butyl [4-chloro-2-((E)-{1-[(4-chlorophenyl)sulfonyl]-3,7-dioxo-1,4-diazepan-6-ylidene}methyl)phenoxy]acetate

Guidance literature:: Multi-step reaction with 5 steps

1.1: NaN₃

1.2: PPh₃; water

2.1: aq. NaOH

3.1: TFA / CH₂Cl₂ / 1 h / 0 °C

4.1: NaI; NaHCO₃ / dimethylformamide / 20 h / 20 °C

With sodium hydroxide; sodium azide; sodium hydrogencarbonate; trifluoroacetic acid; sodium iodide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2007.03.038

Reference yield:

: C₁₅H₂₀ClNO₄

: 889854-32-4
tert-butyl [4-chloro-2-((E)-{1-[(4-chlorophenyl)sulfonyl]-3,7-dioxo-1,4-diazepan-6-ylidene}methyl)phenoxy]acetate

Guidance literature:: Multi-step reaction with 4 steps

1: aq. NaOH

2: TFA / CH₂Cl₂ / 1 h / 0 °C

3: NaI; NaHCO₃ / dimethylformamide / 20 h / 20 °C

With sodium hydroxide; sodium hydrogencarbonate; trifluoroacetic acid; sodium iodide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2007.03.038