Carbamic acid, [(2E)-3-(5-chloro-2-methoxyphenyl)-2-[[[[(4-chlorophenyl)amino]carbonyl ]amino]carbonyl]-2-propenyl]-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Carbamic acid, [(2E)-3-(5-chloro-2-methoxyphenyl)-2-[[[[(4-chlorophenyl)amino]carbonyl ]amino]carbonyl]-2-propenyl]-, 1,1-dimethylethyl ester
CAS No.:889857-21-0
Molecular Formula:C23H25Cl2N3O5
Molecular Weight:494.375
Hs Code.:

Carbamic acid,
[(2E)-3-(5-chloro-2-methoxyphenyl)-2-[[[[(4-chlorophenyl)amino]carbonyl
]amino]carbonyl]-2-propenyl]-, 1,1-dimethylethyl ester

Synonyms:

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Chemical Property of Carbamic acid, [(2E)-3-(5-chloro-2-methoxyphenyl)-2-[[[[(4-chlorophenyl)amino]carbonyl ]amino]carbonyl]-2-propenyl]-, 1,1-dimethylethyl ester

Chemical Property:

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Technology Process of Carbamic acid, [(2E)-3-(5-chloro-2-methoxyphenyl)-2-[[[[(4-chlorophenyl)amino]carbonyl ]amino]carbonyl]-2-propenyl]-, 1,1-dimethylethyl ester

There total 2 articles about Carbamic acid, [(2E)-3-(5-chloro-2-methoxyphenyl)-2-[[[[(4-chlorophenyl)amino]carbonyl ]amino]carbonyl]-2-propenyl]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₉H₂₂ClN₃O₄

: 889857-21-0
tert-butyl (2E)-2-({[(4-chloroanilino)carbonyl]amino}carbonyl)-3-(5-chloro-2-methoxyphenyl)-2-propenylcarbamate

Guidance literature:: N-(4-chlorophenyl)urea; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

C₁₉H₂₂ClN₃O₄; In tetrahydrofuran; N,N-dimethyl-formamide; at 20 ℃; for 16h;

Reference yield:

: 889855-59-8
(2E)-2-{[(tert-butoxycarbonyl)amino]methyl}-3-(5-chloro-2-methoxyphenyl)-2-propenoic acid

: 530-62-1
1,1'-carbonyldiimidazole

: 140-38-5
N-(4-chlorophenyl)urea

: 889857-21-0
tert-butyl (2E)-2-({[(4-chloroanilino)carbonyl]amino}carbonyl)-3-(5-chloro-2-methoxyphenyl)-2-propenylcarbamate

Guidance literature:: N-(4-chlorophenyl)urea; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

(2E)-2-{[(tert-butoxycarbonyl)amino]methyl}-3-(5-chloro-2-methoxyphenyl)-2-propenoic acid; 1,1'-carbonyldiimidazole; In tetrahydrofuran; N,N-dimethyl-formamide; at 0 - 20 ℃; for 16.75h;

Reference yield:

: 22118-09-8
2-bromoacetyl chloride

: 889857-21-0
tert-butyl (2E)-2-({[(4-chloroanilino)carbonyl]amino}carbonyl)-3-(5-chloro-2-methoxyphenyl)-2-propenylcarbamate

: 2-bromo-N-[(2E)-2-({[(4-chloroanilino)carbonyl]amino}carbonyl)-3-(5-chloro-2-methoxyphenyl)-2-propenyl]acetamide

Guidance literature:: tert-butyl (2E)-2-({[(4-chloroanilino)carbonyl]amino}carbonyl)-3-(5-chloro-2-methoxyphenyl)-2-propenylcarbamate; With hydrogenchloride; In water; at 20 ℃; for 1h;

2-bromoacetyl chloride; With triethylamine; In dichloromethane; water; at 0 ℃; for 0.333333h;