Benzoic acid, 3-[(1R,6R)-6-[(5-chloro-2-methoxyphenyl)methyl]-1-ethyl-11,11-dimethyl -3,5,9-trioxo-10-oxa-2,4,8-triazadodec-1-yl]-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Benzoic acid, 3-[(1R,6R)-6-[(5-chloro-2-methoxyphenyl)methyl]-1-ethyl-11,11-dimethyl -3,5,9-trioxo-10-oxa-2,4,8-triazadodec-1-yl]-, 1,1-dimethylethyl ester
CAS No.:889857-67-4
Molecular Formula:C31H42ClN3O7
Molecular Weight:604.143
Hs Code.:

Benzoic acid,
3-[(1R,6R)-6-[(5-chloro-2-methoxyphenyl)methyl]-1-ethyl-11,11-dimethyl
-3,5,9-trioxo-10-oxa-2,4,8-triazadodec-1-yl]-, 1,1-dimethylethyl ester

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Chemical Property of Benzoic acid, 3-[(1R,6R)-6-[(5-chloro-2-methoxyphenyl)methyl]-1-ethyl-11,11-dimethyl -3,5,9-trioxo-10-oxa-2,4,8-triazadodec-1-yl]-, 1,1-dimethylethyl ester

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Technology Process of Benzoic acid, 3-[(1R,6R)-6-[(5-chloro-2-methoxyphenyl)methyl]-1-ethyl-11,11-dimethyl -3,5,9-trioxo-10-oxa-2,4,8-triazadodec-1-yl]-, 1,1-dimethylethyl ester

There total 2 articles about Benzoic acid, 3-[(1R,6R)-6-[(5-chloro-2-methoxyphenyl)methyl]-1-ethyl-11,11-dimethyl -3,5,9-trioxo-10-oxa-2,4,8-triazadodec-1-yl]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 889857-66-3
tert-butyl 3-[(1R)-1-isocyanatepropyl]benzoate

: 889857-67-4
tert-butyl 3-[(1R,6R)-6-(5-chloro-2-methoxybenzyl)-1-ethyl-11,11-dimethyl-3,5,9-trioxo-10-oxa-2,4,8-triazadodec-1-yl]benzoate

Guidance literature:: tert-butyl (2R)-3-amino-2-(5-chloro-2-methoxybenzyl)-3-oxopropylcarbamate; With potassium tert-butylate; In N,N-dimethyl-formamide; at 0 ℃; for 0.25h;

tert-butyl 3-[(1R)-1-isocyanatepropyl]benzoate; In tetrahydrofuran; N,N-dimethyl-formamide; at 0 ℃; for 0.5h;

Reference yield:

: 889857-66-3
tert-butyl 3-[(1R)-1-isocyanatepropyl]benzoate

: 889857-58-3
tert-butyl (2R)-3-amino-2-(5-chloro-2-methoxybenzyl)-3-oxopropylcarbamate

: 889857-67-4
tert-butyl 3-[(1R,6R)-6-(5-chloro-2-methoxybenzyl)-1-ethyl-11,11-dimethyl-3,5,9-trioxo-10-oxa-2,4,8-triazadodec-1-yl]benzoate

Guidance literature:: tert-butyl (2R)-3-amino-2-(5-chloro-2-methoxybenzyl)-3-oxopropylcarbamate; With potassium tert-butylate; In N,N-dimethyl-formamide; at 0 ℃; for 0.25h;

tert-butyl 3-[(1R)-1-isocyanatepropyl]benzoate; In tetrahydrofuran; N,N-dimethyl-formamide; at 0 ℃; for 0.5h;

Reference yield:

: 889857-67-4
tert-butyl 3-[(1R,6R)-6-(5-chloro-2-methoxybenzyl)-1-ethyl-11,11-dimethyl-3,5,9-trioxo-10-oxa-2,4,8-triazadodec-1-yl]benzoate

: C₂₆H₃₄ClN₃O₅

Guidance literature:: tert-butyl 3-[(1R,6R)-6-(5-chloro-2-methoxybenzyl)-1-ethyl-11,11-dimethyl-3,5,9-trioxo-10-oxa-2,4,8-triazadodec-1-yl]benzoate; With hydrogenchloride; In ethyl acetate; at 0 - 20 ℃; for 6h;

With sodium hydroxide; In water; ethyl acetate; at 0 ℃;