3a-Methyl-2-phenyl-4,5,6,7-tetrahydro-3aH-benzimidazole

Base Information

Chemical Name:3a-Methyl-2-phenyl-4,5,6,7-tetrahydro-3aH-benzimidazole
CAS No.:89002-64-2
Molecular Formula:C₁₄H₁₆N₂
Molecular Weight:212.294
Hs Code.:
DSSTox Substance ID:DTXSID20550830

Synonyms:89002-64-2;3a-Methyl-2-phenyl-4,5,6,7-tetrahydro-3aH-benzimidazole;DTXSID20550830

Suppliers and Price of 3a-Methyl-2-phenyl-4,5,6,7-tetrahydro-3aH-benzimidazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 3a-Methyl-2-phenyl-4,5,6,7-tetrahydro-3aH-benzimidazole

Chemical Property:

XLogP3:2.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:212.131348519
Heavy Atom Count:16
Complexity:337

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC12CCCCC1=NC(=N2)C3=CC=CC=C3

Technology Process of 3a-Methyl-2-phenyl-4,5,6,7-tetrahydro-3aH-benzimidazole

There total 4 articles about 3a-Methyl-2-phenyl-4,5,6,7-tetrahydro-3aH-benzimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 89002-62-0
1-(2-methylcyclohex-1-enyl)-5-phenyltetrazole

: 89002-64-2
3a-methyl-2-phenyl-4,5,6,7-tetrahydro-3aH-benzimidazole

: 112081-43-3
8a-methyl-4a,5,6,7,8,8a-hexahydrotetrazolo<1,5-f>phenanthridine

Guidance literature:: In Petroleum ether; for 3h; Irradiation;

Reference yield:

: 112081-46-6,112081-47-7
1-<(1RS,2SR)-2-hydroxy-2-methylcyclohexyl>-5-phenyltetrazole

: 89002-64-2
3a-methyl-2-phenyl-4,5,6,7-tetrahydro-3aH-benzimidazole

Guidance literature:: Multi-step reaction with 2 steps

1: 19 percent / POCl₃ / pyridine / 1.5 h

2: 41 percent / acetonitrile / 2.5 h / Irradiation

With trichlorophosphate; In pyridine; acetonitrile;

Reference yield:

: 83576-18-5
1-(2-hydroxycyclohexyl)-5-phenyltetrazole

: 89002-64-2
3a-methyl-2-phenyl-4,5,6,7-tetrahydro-3aH-benzimidazole

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / benzene / 3 h / Heating

2: 19 percent / POCl₃ / pyridine / 1.5 h

3: 41 percent / acetonitrile / 2.5 h / Irradiation

With trichlorophosphate; In pyridine; acetonitrile; benzene;