Benzenehexanoyl chloride, 4-chloro-

Base Information

Chemical Name:Benzenehexanoyl chloride, 4-chloro-
CAS No.:89007-39-6
Molecular Formula:C12H14Cl2O
Molecular Weight:245.149
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenehexanoyl chloride, 4-chloro-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzenehexanoyl chloride, 4-chloro-

There total 5 articles about Benzenehexanoyl chloride, 4-chloro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54887-73-9
6-(4-chlorophenyl)hexanoic acid

: 89007-39-6
6-(p-chlorophenyl)hexanoic acid chloride

Guidance literature:: With thionyl chloride; In benzene;

Reference yield:

: 104-88-1
4-chlorobenzaldehyde

: 89007-39-6
6-(p-chlorophenyl)hexanoic acid chloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / 1.75 h / -78 - 0 °C / Inert atmosphere

1.2: 18 h / Inert atmosphere

2.1: hydrogen; palladium 10% on activated carbon / methanol / 2 h / 20 °C

3.1: N,N-dimethyl-formamide; oxalyl dichloride / 1 h / Inert atmosphere

With oxalyl dichloride; palladium 10% on activated carbon; hydrogen; N,N-dimethyl-formamide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; 1.1: |Wittig Olefination / 1.2: |Wittig Olefination;
DOI:10.1016/j.ejmech.2017.08.004

Reference yield:

: C₁₂H₁₃ClO₂

: 89007-39-6
6-(p-chlorophenyl)hexanoic acid chloride

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen; palladium 10% on activated carbon / methanol / 2 h / 20 °C

2: N,N-dimethyl-formamide; oxalyl dichloride / 1 h / Inert atmosphere

With oxalyl dichloride; palladium 10% on activated carbon; hydrogen; N,N-dimethyl-formamide; In methanol;
DOI:10.1016/j.ejmech.2017.08.004