Stannane, (1-iodo-2-phenylethenyl)trimethyl-, (E)-

Base Information

Chemical Name:Stannane, (1-iodo-2-phenylethenyl)trimethyl-, (E)-
CAS No.:89029-51-6
Molecular Formula:C₁₁H₁₅ISn
Molecular Weight:392.855
Hs Code.:

Synonyms:

Suppliers and Price of Stannane, (1-iodo-2-phenylethenyl)trimethyl-, (E)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Stannane, (1-iodo-2-phenylethenyl)trimethyl-, (E)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Stannane, (1-iodo-2-phenylethenyl)trimethyl-, (E)-

There total 3 articles about Stannane, (1-iodo-2-phenylethenyl)trimethyl-, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 89029-57-2,89029-51-6
(E)-PhCH=CISnMe₃

: 89029-51-6,89029-57-2
(Z)-PhCH=CISnMe₃

Guidance literature:: With magnesium; In tetrahydrofuran; Ar-atmosphere; 70°C, 20 h; not isolated, detd. by (1)H-NMR spectroscopy;
DOI:10.1016/S0022-328X(00)99294-5

Reference yield:

: 78338-47-3
C₆H₅CHC(Sn(CH₃)3)2

: 89029-57-2,89029-51-6
(E)-PhCH=CISnMe₃

: 89029-51-6,89029-57-2
(Z)-PhCH=CISnMe₃

Guidance literature:: With iodine; In chloroform; byproducts: PhCH=CI2; Ar-atmosphere; slow addn. of 2 equivs. I2 to Sn-compd. (-78 or 20°C), stirring (1 h, room temp.); distn. off of CHCl3 (normal pressure); isomer mixt. not sepd., detd. by(1)H- and (13)C-NMR spectroscopy (isomer ratio depending on reaction temp.); total yield 76%;
DOI:10.1016/S0022-328X(00)99294-5

Reference yield:

: 78338-47-3
C₆H₅CHC(Sn(CH₃)3)2

: 89029-57-2,89029-51-6
(E)-PhCH=CISnMe₃

: 89029-51-6,89029-57-2
(Z)-PhCH=CISnMe₃

Guidance literature:: With iodine; In chloroform; byproducts: PhCH=CI2; Ar-atmosphere; slow addn. of 2 equivs. I2 to Sn-compd. (-78 or 20°C), stirring (1 h, room temp.); distn. off of CHCl3 (normal pressure); isomer mixt. not sepd., detd. by(1)H- and (13)C-NMR spectroscopy (isomer ratio depending on reaction temp.); total yield 76%;
DOI:10.1016/S0022-328X(00)99294-5