1,3,6-Trimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde

Base Information

Chemical Name:1,3,6-Trimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde
CAS No.:23941-84-6
Molecular Formula:C8H10 N2 O3
Molecular Weight:182.179
Hs Code.:2933599090
DSSTox Substance ID:DTXSID70946764
Nikkaji Number:J498.591E
Wikidata:Q82924447
Mol file:23941-84-6.mol

Synonyms:23941-84-6;1,3,6-trimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde;1,3,6-Trimethyl-2,4-dioxo-1,2,3,4-tetrahydro-pyrimidine-5-carbaldehyde;1,3,4-trimethyl-2,6-dioxopyrimidine-5-carbaldehyde;SCHEMBL3791186;DTXSID70946764;YAA94184;AKOS000662937;SB55660;CS-0358020;FT-0690853

Suppliers and Price of 1,3,6-Trimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
1,3,6-Trimethyl-2,4-dioxo-1,2,3,4-tetrahydro-pyrimidine-5-carbaldehyde
1g
$ 378.00

Crysdot
1,3,6-Trimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde 95+%
5g
$ 749.00

Chemenu
1,3,6-Trimethyl-2,4-dioxo-1,2,3,4-tetrahydro-pyrimidine-5-carbaldehyde 95%
5g
$ 707.00

American Custom Chemicals Corporation
1,3,6-TRIMETHYL-2,4-DIOXO-1,2,3,4-TETRAHYDRO-PYRIMIDINE-5-CARBALDEHYDE 95.00%
500MG
$ 762.30

Total 10 raw suppliers

Chemical Property of 1,3,6-Trimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde

Chemical Property:

Vapor Pressure:0.00321mmHg at 25°C
Boiling Point:283.2°Cat760mmHg
PKA:-3.02±0.60(Predicted)
Flash Point:123°C
PSA：61.07000
Density:1.325g/cm³
LogP:-0.79510
Storage Temp.:2-8°C
XLogP3:-0.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:182.06914219
Heavy Atom Count:13
Complexity:319

Purity/Quality:

97% ^*data from raw suppliers

1,3,6-Trimethyl-2,4-dioxo-1,2,3,4-tetrahydro-pyrimidine-5-carbaldehyde ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xi
Hazard Codes:Xi

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C(=O)N(C(=O)N1C)C)C=O

Technology Process of 1,3,6-Trimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde

There total 4 articles about 1,3,6-Trimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 13509-52-9
1,3,6-trimethyluracil

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 23941-84-6
5-formy-1,3,6-trimethyluracil

Guidance literature:: With trichlorophosphate; at 0 - 120 ℃; for 4h; Inert atmosphere;
DOI:10.1002/anie.202007509

Reference yield:

: 626-48-2
6-Methyluracil

: 23941-84-6
5-formy-1,3,6-trimethyluracil

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / acetone / 0.5 h / 20 °C / Inert atmosphere

1.2: 8 h / 60 °C / Inert atmosphere

2.1: trichlorophosphate / 4 h / 0 - 120 °C / Inert atmosphere

With potassium carbonate; trichlorophosphate; In acetone;
DOI:10.1002/anie.202007509