1-(Bromomethyl)-2,3,4,5-tetramethoxy-6-methylbenzene

Base Information

Chemical Name:1-(Bromomethyl)-2,3,4,5-tetramethoxy-6-methylbenzene
CAS No.:89048-14-6
Molecular Formula:C12H17BrO4
Molecular Weight:305.169
Hs Code.:
DSSTox Substance ID:DTXSID60564714
Nikkaji Number:J3.450.445H
Wikidata:Q82449519

Synonyms:89048-14-6;1-(Bromomethyl)-2,3,4,5-tetramethoxy-6-methylbenzene;SCHEMBL7971435;DTXSID60564714;PJLFSVSXQYHYAN-UHFFFAOYSA-N;1,2,3,4-tetramethoxy-5-methyl-6-bromomethylbenzene;1,2,3,4-tetramethoxy-5-methyl-6-bromomethyl-benzene;5-Bromomethyl-1,2,3,4-tetramethoxy-6-methylbenzene

Suppliers and Price of 1-(Bromomethyl)-2,3,4,5-tetramethoxy-6-methylbenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1-(Bromomethyl)-2,3,4,5-tetramethoxy-6-methylbenzene

Chemical Property:

XLogP3:2.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:304.03102
Heavy Atom Count:17
Complexity:227

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C(=C(C(=C1OC)OC)OC)OC)CBr

Technology Process of 1-(Bromomethyl)-2,3,4,5-tetramethoxy-6-methylbenzene

There total 10 articles about 1-(Bromomethyl)-2,3,4,5-tetramethoxy-6-methylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 35896-58-3
2,3,4,5-tetramethoxytoluene

: 89048-14-6
1-(bromomethyl)-2,3,4,5-tetramethoxy-6-methylbenzene

Guidance literature:: With hydrogen bromide; at 40 ℃; for 1h;
DOI:10.1016/j.bioorg.2016.08.008

Reference yield: 98.0%

: 35896-58-3
2,3,4,5-tetramethoxytoluene

: 123-63-7
paracetaldehyde

: 89048-14-6
1-(bromomethyl)-2,3,4,5-tetramethoxy-6-methylbenzene

Guidance literature:: With hydrogen bromide; In water; at 40 ℃; for 1h;
DOI:10.3184/174751914X14024185967888

Reference yield:

: 3066-90-8
2,3-dimethoxy-5-methylbenzene-1,4-diol

: 89048-14-6
1-(bromomethyl)-2,3,4,5-tetramethoxy-6-methylbenzene

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide / ethanol; water / 0 - 20 °C

2: titanium tetrachloride / dichloromethane / 0 - 20 °C

3: potassium borohydride / ethanol / 0.5 h / 0 °C

4: phosphorus tribromide / tetrahydrofuran / 0.5 h / 0 °C

With potassium borohydride; phosphorus tribromide; titanium tetrachloride; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1021/ja204014s